3,3-二甲基-1-丁烯合成路线 (共 347 条)
反应条件
hydrogen; methanesulfonic acid; lt;Pt(C2H4)(DPPB)gt; in toluene T=100°C; P=38000 Torr; var. olefins; Product distribution;
参考文献
Botteghi, Carlo; Paganelli, Stefano
Journal of Organometallic Chemistry, 1991 , vol. 417, # 1/2 p. C41 - C45
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=200°C; 24 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
carbon monoxide; palladium on activated charcoal; 1,4-di(diphenylphosphino)-butane in ethylene glycol dimethyl ether T=150°C; P=5168 Torr; 24 h;
参考文献
Ali, B. El; Vasapollo, G.; Alper, H.
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4739 - 4741
反应条件
carbon monoxide; palladium on activated charcoal; 1,4-di(diphenylphosphino)-butane in ethylene glycol dimethyl ether T=150°C; P=30400 Torr; 24 h;
参考文献
Ali, B. El; Vasapollo, G.; Alper, H.
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4739 - 4741
反应条件
mercury(II) diacetate in tetrahydrofuran; water 1 h; Ambient temperatureother mercuri salts, other reaction time; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 46, # 19 p. 3810 - 3812
反应条件
anhydrous sodium borate; aluminium trichloride; triglyme (triethylene glycol dimethyl ether) anschliessend mit wss.Wasserstoffperoxid und wss.Natronlauge;
参考文献
Delacre
Chem. Zentralbl., 1906 , vol. 77, # I p. 1233
反应条件
triphenyl phosphite; Ni[P(OPh)3]4; zinc(II) chloride in toluene T=60°C; 2.5 h;
参考文献
Jackson, W. Roy; Lovel, Craig G.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2053 - 2067
反应条件
copper diacetate; bis(cyclohexanyl)borane; bis(acetylacetonato)copper(II) in tetrahydrofuran
参考文献
Masuda, Yuzuru; Hoshi, Masayuki; Arase, Akira
Journal of the Chemical Society, Chemical Communications, 1989 , # 5 p. 266 - 267
反应条件
Yield given. Multistep reaction;
参考文献
Buchwald, Stephen L.; LaMaire, Susan J.
Tetrahedron Letters, 1987 , vol. 28, # 3 p. 295 - 298
反应条件
Yield given. Multistep reaction;
参考文献
Buchwald, Stephen L.; LaMaire, Susan J.
Tetrahedron Letters, 1987 , vol. 28, # 3 p. 295 - 298