3,3-二甲基-1-丁烯合成路线 （共 347 条）
参考文献
Collier,W.L.; Macomber,R.S.
Journal of Organic Chemistry, 1973 , vol. 38, p. 1367 - 1369
参考文献
Trahanovsky,W.S.; Himstedt,A.L.
Journal of the American Chemical Society, 1974 , vol. 96, p. 7974 - 7976
参考文献
Collier,W.L.; Macomber,R.S.
Journal of Organic Chemistry, 1973 , vol. 38, p. 1367 - 1369
参考文献
Delacre
Chem. Zentralbl., 1906 , vol. 77, # II p. 1233
反应条件
copper(l) iodide; chloro-trimethyl-silane; zinc(II) chloride; zinc in diethyl ether 22 h; Inert atmosphereReflux; diastereoselective reaction;
参考文献
Begis, Guillaume; Cladingboel, David E.; Jerome, Laure; Motherwell, William B.; Sheppard, Tom D.
European Journal of Organic Chemistry, 2009 , # 10 p. 1532 - 1548
反应条件
in tetrachloromethane; dichloromethane T=14 - 15°C; 0.25 h; Irradiation; Yields of byproduct given;
参考文献
Tlumak, Robert L.; Day, James C.; Slanga, Joseph P.; Skell, Philip S.
Journal of the American Chemical Society, 1982 , vol. 104, # 25 p. 7257 - 7267
反应条件
neopentane2,2-dimethylpropane; dichloromethane; [14C]-1,1-Dichloroethylene T=14 - 15°C; 1 h; Irradiationfree-radical isomerization of N-bromosuccinimide to β-bromopropionyl isocyanate, photolysis in the presence of halogen scavengers, halogens; dependence on NBS concentration, effect of alkenes; isomerization of other succinimides and glutarimides; Product distributionRate constant;
参考文献
Tlumak, Robert L.; Day, James C.; Slanga, Joseph P.; Skell, Philip S.
Journal of the American Chemical Society, 1982 , vol. 104, # 25 p. 7257 - 7267
反应条件
1: dibenzoyl peroxide; HBr 2: NH3 / 106 - 120 °C / 51485.6 - 66195.7 Torr View Scheme
参考文献
Howe; Hass
Industrial and Engineering Chemistry, 1946 , vol. 38, p. 252
反应条件
1: 50 percent / aq. magnesium monoperphthalate hexahydrate / propan-2-ol / 12 h / 20 °C 2: n-BuLi; 2,2,6,6-tetramethylpiperidine / tetrahydrofuran; cyclohexane / 15 h / 20 °C View Scheme
参考文献
Katritzky, Alan R.; Fang, Yunfeng; Prakash, Indra
Journal of the Indian Chemical Society, 2000 , vol. 77, # 11-12 p. 635 - 636
反应条件
dimethylsulfide borane complex; pyridinium chlorochromate 1.) CH2Cl2, 1 h, RT; 2.) CH2Cl2, reflux, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Brown, Herbert C.; Kulkarni, Surendra U.; Rao, C. Gundu; Patil, Vemanna D.
Tetrahedron, 1986 , vol. 42, # 20 p. 5515 - 5522
