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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
吡吲醇菌素
合成路线
（共 17 条）
1443051-70-4
→
反应条件
55812-46-9
吡吲醇菌素
反应条件
hydrogenchloride in tetrahydrofuran; water T=0°C; 2 h;
参考文献
Zhang, Qiang; Fan, Zhen; Dong, Jing; Shi, Xiao-Xin; Lu, Xia
Tetrahedron Asymmetry, 2013 , vol. 24, # 11 p. 633 - 637
189756-51-2
→
反应条件
55812-46-9
吡吲醇菌素
反应条件
potassium carbonate in methanol T=20°C; 1 h;
参考文献
Kanekiyo; Kuwada; Choshi; Nobuhiro; Hibino
Journal of Organic Chemistry, 2001 , vol. 66, # 26 p. 8793 - 8798
188037-57-2
→
反应条件
55812-46-9
吡吲醇菌素
反应条件
1: 97 percent / Et4NCl / PdCl2(PPh3)2 / dimethylformamide / 0.67 h / 80 °C 2: 93 percent / NH2OH*HCl; AcONa / ethanol / 0.5 h / 80 °C 3: 95 percent / 1,2-dichloro-benzene / 0.33 h / 180 °C 4: 90 percent / Ac2O / 3 h / 100 °C 5: 99 percent / pyridine; CH2Cl2 / 0.17 h / 20 °C 6: 72 percent / Et4NCl / PdCl2(PPh3)2 / dimethylformamide / 0.67 h / 80 °C 7: 93 percent / CF3SO3H; CH(OMe)3 / methanol; nitromethane / 1 h / 100 °C 8: 98 percent / pyridine / 2 h / 20 °C 9: 68 percent / AD-mix-β / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C 10: 93 percent / 1 M K2CO3 / methanol / 1 h / 20 °C View Scheme
参考文献
Kanekiyo; Kuwada; Choshi; Nobuhiro; Hibino
Journal of Organic Chemistry, 2001 , vol. 66, # 26 p. 8793 - 8798
67-56-1
甲醇
+
124-41-4
甲醇钠
+
189756-51-2
→
反应条件
55812-46-9
吡吲醇菌素
反应条件
in methanol T=25°C; Hydrolysis; 1 h;
参考文献
Kim, Yong-Pil; Takamatsu, Satoshi; Hayashi, Masahiko; Komiyama, Kanki; Omura, Satoshi
Journal of Antibiotics, 1997 , vol. 50, # 3 p. 189 - 193
67-56-1
甲醇
+
124-41-4
甲醇钠
+
189756-49-8
→
反应条件
55812-46-9
吡吲醇菌素
反应条件
in methanol T=25°C; Hydrolysis; 1 h;
参考文献
Kim, Yong-Pil; Takamatsu, Satoshi; Hayashi, Masahiko; Komiyama, Kanki; Omura, Satoshi
Journal of Antibiotics, 1997 , vol. 50, # 3 p. 189 - 193
304435-38-9
→
反应条件
55812-46-9
吡吲醇菌素
反应条件
1: 93 percent / NH2OH*HCl; AcONa / ethanol / 0.5 h / 80 °C 2: 95 percent / 1,2-dichloro-benzene / 0.33 h / 180 °C 3: 90 percent / Ac2O / 3 h / 100 °C 4: 99 percent / pyridine; CH2Cl2 / 0.17 h / 20 °C 5: 72 percent / Et4NCl / PdCl2(PPh3)2 / dimethylformamide / 0.67 h / 80 °C 6: 93 percent / CF3SO3H; CH(OMe)3 / methanol; nitromethane / 1 h / 100 °C 7: 98 percent / pyridine / 2 h / 20 °C 8: 68 percent / AD-mix-β / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C 9: 93 percent / 1 M K2CO3 / methanol / 1 h / 20 °C View Scheme
参考文献
Kanekiyo; Kuwada; Choshi; Nobuhiro; Hibino
Journal of Organic Chemistry, 2001 , vol. 66, # 26 p. 8793 - 8798
304435-40-3
→
反应条件
55812-46-9
吡吲醇菌素
反应条件
1: 90 percent / Ac2O / 3 h / 100 °C 2: 99 percent / pyridine; CH2Cl2 / 0.17 h / 20 °C 3: 72 percent / Et4NCl / PdCl2(PPh3)2 / dimethylformamide / 0.67 h / 80 °C 4: 93 percent / CF3SO3H; CH(OMe)3 / methanol; nitromethane / 1 h / 100 °C 5: 98 percent / pyridine / 2 h / 20 °C 6: 68 percent / AD-mix-β / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C 7: 93 percent / 1 M K2CO3 / methanol / 1 h / 20 °C View Scheme
参考文献
Kanekiyo; Kuwada; Choshi; Nobuhiro; Hibino
Journal of Organic Chemistry, 2001 , vol. 66, # 26 p. 8793 - 8798
304435-39-0
→
反应条件
55812-46-9
吡吲醇菌素
反应条件
1: 95 percent / 1,2-dichloro-benzene / 0.33 h / 180 °C 2: 90 percent / Ac2O / 3 h / 100 °C 3: 99 percent / pyridine; CH2Cl2 / 0.17 h / 20 °C 4: 72 percent / Et4NCl / PdCl2(PPh3)2 / dimethylformamide / 0.67 h / 80 °C 5: 93 percent / CF3SO3H; CH(OMe)3 / methanol; nitromethane / 1 h / 100 °C 6: 98 percent / pyridine / 2 h / 20 °C 7: 68 percent / AD-mix-β / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C 8: 93 percent / 1 M K2CO3 / methanol / 1 h / 20 °C View Scheme
参考文献
Kanekiyo; Kuwada; Choshi; Nobuhiro; Hibino
Journal of Organic Chemistry, 2001 , vol. 66, # 26 p. 8793 - 8798
304435-42-5
→
反应条件
55812-46-9
吡吲醇菌素
反应条件
1: 72 percent / Et4NCl / PdCl2(PPh3)2 / dimethylformamide / 0.67 h / 80 °C 2: 93 percent / CF3SO3H; CH(OMe)3 / methanol; nitromethane / 1 h / 100 °C 3: 98 percent / pyridine / 2 h / 20 °C 4: 68 percent / AD-mix-β / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C 5: 93 percent / 1 M K2CO3 / methanol / 1 h / 20 °C View Scheme
参考文献
Kanekiyo; Kuwada; Choshi; Nobuhiro; Hibino
Journal of Organic Chemistry, 2001 , vol. 66, # 26 p. 8793 - 8798
392716-47-1
→
反应条件
55812-46-9
吡吲醇菌素
反应条件
1: 89 percent / mCPBA / CH2Cl2 / 2 h / 20 °C 2: 90 percent / Ac2O / 3 h / 100 °C 3: 99 percent / pyridine; CH2Cl2 / 0.17 h / 20 °C 4: 72 percent / Et4NCl / PdCl2(PPh3)2 / dimethylformamide / 0.67 h / 80 °C 5: 93 percent / CF3SO3H; CH(OMe)3 / methanol; nitromethane / 1 h / 100 °C 6: 98 percent / pyridine / 2 h / 20 °C 7: 68 percent / AD-mix-β / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C 8: 93 percent / 1 M K2CO3 / methanol / 1 h / 20 °C View Scheme
参考文献
Kanekiyo; Kuwada; Choshi; Nobuhiro; Hibino
Journal of Organic Chemistry, 2001 , vol. 66, # 26 p. 8793 - 8798
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