反应条件
1: (+/-)-2,2-dimethyl-5-phenyl-1,3-dioxolan-4-one With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
T=-78°C; 0.5 h;
2: 8‐iodo‐2,6‐dimethyloct‐2‐ene With N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran; hexane
T=-78 - 20°C; 4 h;
参考文献
Blay, Gonzalo; Fernandez, Isabel; Monje, Belen; Pedro, Jose R.
Molecules, 2004 , vol. 9, # 5 p. 365 - 372
