反应条件
1: 90 percent / potassium carbonate / ethanol; H2O / 0.5 h / Heating
2: 1) m-(chloroperoxy)benzoic acid, 2) triethylamine, acetic anhydride / 1) diethyl ether/dichloromethane, 0 to 20 deg C, 2 h, 2) CH2Cl2, 0 deg C, 30 min
3: 90 percent / 10percent aq. sulfuric acid / ethanol / 4 h / 20 °C
View Scheme
参考文献
Kuehne, Martin E.; Muth, Randy S.
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2701 - 2712
