4-异丙基苯基二苯基磷酸酯合成路线 （共 8 条）
反应条件
trichlorophosphate; magnesium chloride
T=130 - 230°C; 2 h;
参考文献
Albemarle Corporation
Patent: US2012/4438 A1, 2012 ;
Location in patent: Page/Page column 8 ;
反应条件
trichlorophosphate; magnesium chloride
T=130 - 230°C; 2 h;
参考文献
Albemarle Corporation
Patent: US2012/4438 A1, 2012 ;
Location in patent: Page/Page column 8 ;
反应条件
1.1: Amberlyst.(R). 15 / 110 - 118 °C / 2311.54 - 4897.34 Torr / Autoclave; Inert atmosphere
2.1: trichlorophosphate; tetrabutylammomium bromide / 114 °C
2.2: 9 h / 110 - 130 °C / Inert atmosphere
View Scheme
参考文献
Albemarle Corporation
Patent: US2012/4438 A1, 2012 ;
反应条件
1: Amberlyst.(R). 15 / 110 - 118 °C / 2311.54 - 4897.34 Torr / Autoclave; Inert atmosphere
2: trichlorophosphate / magnesium chloride / 2 h / 130 - 230 °C
View Scheme
参考文献
Albemarle Corporation
Patent: US2012/4438 A1, 2012 ;
反应条件
1: With tetrabutylammomium bromide; trichlorophosphate
T=114°C;
2: With magnesium chloride
T=110 - 130°C; 9 h; Inert atmosphere; Product distribution / selectivity;
参考文献
Albemarle Corporation
Patent: US2012/4438 A1, 2012 ;
Location in patent: Page/Page column 8-9 ;
反应条件
1: Amberlyst.(R). 15 / 110 - 118 °C / 2311.54 - 4897.34 Torr / Autoclave; Inert atmosphere
2: trichlorophosphate / magnesium chloride / 2 h / 130 - 230 °C
View Scheme
参考文献
Albemarle Corporation
Patent: US2012/4438 A1, 2012 ;
反应条件
1: With tetrabutylammomium bromide; trichlorophosphate
T=114 - 135°C;
2: With magnesium chloride
T=110 - 135°C; 3 h; Product distribution / selectivity;
参考文献
Albemarle Corporation
Patent: US2012/4438 A1, 2012 ;
Location in patent: Page/Page column 10 ;
参考文献
Honkakoski, Paavo; Palvimo, Jorma J.; Penttilae, Leena; Vepsaelaeinen, Jouko; Auriola, Seppo
Biochemical Pharmacology, 2004 , vol. 67, # 1 p. 97 - 106
