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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
55877-36-6
合成路线
（共 6 条）
55877-35-5
→
反应条件
55877-36-6
反应条件
pyridine hydrochloride T=200°C; 2 h;
参考文献
Durani, N.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 5 p. 489 - 490
2491-32-9
苄基-4-羟基苯酮
→
反应条件
55877-36-6
反应条件
1: 100 percent / HCl (gas) / ethyl acetate; ethanol / 1.) 0 deg C, 15 min, 2.) overnight 2: 75 percent / conc. H2SO4, 30 percent H2O2 / methanol / 0 °C 3: 80 percent / KOH / aq. ethanol / 10 h / Heating 4: 25 percent / aq. HCl, HOAc / 10 h / Heating 5: 75 percent / pyridine hydrochloride / 2 h / 200 °C View Scheme
参考文献
Durani, N.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 5 p. 489 - 490
57664-48-9
→
反应条件
55877-36-6
反应条件
1: 80 percent / KOH / aq. ethanol / 10 h / Heating 2: 25 percent / aq. HCl, HOAc / 10 h / Heating 3: 75 percent / pyridine hydrochloride / 2 h / 200 °C View Scheme
参考文献
Durani, N.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 5 p. 489 - 490
87444-82-4
→
反应条件
55877-36-6
反应条件
1: 75 percent / conc. H2SO4, 30 percent H2O2 / methanol / 0 °C 2: 80 percent / KOH / aq. ethanol / 10 h / Heating 3: 25 percent / aq. HCl, HOAc / 10 h / Heating 4: 75 percent / pyridine hydrochloride / 2 h / 200 °C View Scheme
参考文献
Durani, N.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 5 p. 489 - 490
90-02-8
水杨醛
→
反应条件
55877-36-6
反应条件
1: 100 percent / HCl (gas) / ethyl acetate; ethanol / 1.) 0 deg C, 15 min, 2.) overnight 2: 75 percent / conc. H2SO4, 30 percent H2O2 / methanol / 0 °C 3: 80 percent / KOH / aq. ethanol / 10 h / Heating 4: 25 percent / aq. HCl, HOAc / 10 h / Heating 5: 75 percent / pyridine hydrochloride / 2 h / 200 °C View Scheme
参考文献
Durani, N.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 5 p. 489 - 490
57664-47-8
→
反应条件
55877-36-6
反应条件
1: 25 percent / aq. HCl, HOAc / 10 h / Heating 2: 75 percent / pyridine hydrochloride / 2 h / 200 °C View Scheme
参考文献
Durani, N.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 5 p. 489 - 490
