二(二甲基乙烯亚基)焦磷酸酯合成路线 (共 15 条)
反应条件
phosgene; tetrabutyl-ammonium chloride in benzene T=20°C;
参考文献
Ramirez, Fausto; Marecek, James F.
Journal of Organic Chemistry, 1983 , vol. 48, # 6 p. 847 - 850
反应条件
2,4,6-trimethyl-pyridine in dichloromethane
参考文献
Ramirez,F. et al.
Journal of the American Chemical Society, 1976 , vol. 98, # 17 p. 5310 - 5319
参考文献
Ramirez,F. et al.
Synthesis, 1975 , p. 99 - 100
反应条件
phosgene in dichloromethane
T=0°C; 0.5 h;
参考文献
Ramirez, Fausto; Marecek, James F.
Journal of Organic Chemistry, 1983 , vol. 48, # 6 p. 847 - 850
反应条件
tetrafluorodiphospate
> 60 deg C;
参考文献
Ugi, I.; Schwarz, R.
Angewandte Chemie, 1981 , vol. 93, # 9 p. 836 - 838
反应条件
in chloroform-d1
T=37°C; Product distribution;
参考文献
Ramirez, Fausto; Ricci, John S.; Okazaki, Hiroshi; Marecek, James F.; Lewy, Mark
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 20, p. 279 - 300
反应条件
2,3,5-trimethyl-pyridine in dichloromethane
参考文献
Ramirez,F. et al.
Synthesis, 1975 , p. 99 - 100
反应条件
2,3,5-trimethyl-pyridine in dichloromethane
参考文献
Ramirez,F. et al.
Journal of Organic Chemistry, 1977 , vol. 42, p. 771 - 778
反应条件
(i)Et3N, (ii) /BRN= 1730878/, Et3N; Multistep reaction;
参考文献
Ramirez,F. et al.
Journal of the American Chemical Society, 1976 , vol. 98, # 17 p. 5310 - 5319
反应条件
2,3,5-trimethyl-pyridine in dichloromethane
参考文献
Ramirez,F. et al.
Journal of Organic Chemistry, 1977 , vol. 42, p. 771 - 778