2-异丙基-2,3-二甲基丁腈合成路线 (共 8 条)
反应条件
sodium amide in ammonia
参考文献
Journal of the American Chemical Society, , vol. 82, p. 873 - 875
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide in tetrahydrofuran T=0°C; 2 h; effect of temp. and steric parameters on alkylation yields; further alkyl iodides; Product distribution;
参考文献
Tetrahedron, , vol. 36, p. 775 - 778
反应条件
(i) NaNH2, liq. NH3, (ii) /BRN= 1209223/; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 82, p. 873 - 875
参考文献
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, , vol. 280, p. 889 - 892
反应条件
PPA T=140°C; Ritter-type reaction; 10 h;
参考文献
Lebedev, Mikhail Y.; Erman, Mark B.
Tetrahedron Letters, 2002 , vol. 43, # 8 p. 1397 - 1399
反应条件
sulfuric acid; acetic acid T=100°C; Ritter-type reaction; 47 h; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Lebedev, Mikhail Y.; Erman, Mark B.
Tetrahedron Letters, 2002 , vol. 43, # 8 p. 1397 - 1399
反应条件
1: aqueous sulfuric acid / 140 °C 2: sodium nitrite; aqueous sulfuric acid View Scheme
参考文献
Tsai et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 2530
参考文献
Millennium Specialty Chemicals
Patent: US6482983 B1, 2002 ;