lithium aluminium tetrahydride in diethyl ether; benzene 6 h; Heating;

potassium hydroxide in ethanol; water 16 h; Heating;

1: 94.6 percent / lithium aluminium hydride / diethyl ether; benzene / 6 h / Heating 2: 86 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature View Scheme

hydrogen; nickel in n-heptane T=90°C; P=76000.1 Torr; 5 h;

borohydride exchange resin; nickel diacetate in methanol T=20°C; 9 h;

pyridine; trichloroisocyanuric acid in acetonitrile

1: dimethyl lt;1-(methoxycarbonyl)ethylgt;phosphonate With sodium hydride in tetrahydrofuran; mineral oil T=0 - 40°C; Horner-Wadsworth-Emmons olefination; 2: pelargonaldehyde in tetrahydrofuran; mineral oil Horner-Wadsworth-Emmons olefination; 24 h; Reflux; 3: With platinum(IV) oxide; hydrogen in methanol

oxygen; copper dichloride; palladium dichloride T=25°C; 23 h; var. palladium catalysts, solvents and reaction times; Product distribution;

T=30°C; Rate constant;