(4E)-1,4-十一碳二烯合成路线 （共 20 条）
反应条件
hydrogen iodide in benzene
参考文献
Uchida,K. et al.
Journal of Organic Chemistry, 1976 , vol. 41, p. 2215 - 2217
反应条件
1: (i) iBu2AlH, heptane, (ii) MeLi, ether, (iii) /BRN= 635704/
2: aq. HI / benzene
View Scheme
参考文献
Uchida,K. et al.
Journal of Organic Chemistry, 1976 , vol. 41, p. 2215 - 2217
反应条件
perchloric acid in diethyl ether
T=0°C; 0.0833333 h; other <2-<(trimethylsilyl)methyl>cyclopropyl>carbinols, var. reagents; stereoselective formation of cis and trans olefins; Product distributionMechanism;
参考文献
Wilson, Stephen R.; Zucker, Paul A.
Journal of Organic Chemistry, 1988 , vol. 53, # 20 p. 4682 - 4693
反应条件
(i) iBu2AlH, (ii) /BRN= 605308/, CuCl; Multistep reaction;
参考文献
Lynd,R.A.; Zweifel,G.
Synthesis, 1974 , p. 658 - 659
反应条件
sodium hydroxide; carbon monoxide; sodium palladate
2.) water, 0 deg C, 30 min;
参考文献
Miyaura, Norio; Yano, Takashi; Suzuki, Akira
Tetrahedron Letters, 1980 , vol. 21, p. 2865 - 2868
反应条件
acetic acid; 2-propenylmagnesium bromide
1) THF, -50 deg C, 1 h, 2) RT, 3 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Arase; Hoshi; Masuda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 209 - 213
反应条件
sodium hydroxide; copper(l) iodide; methyllithium; dihydrogen peroxide
Yield given. Multistep reaction;
参考文献
Miyaura, Norio; Yano, Takashi; Suzuki, Akira
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 5 p. 1471 - 1472
反应条件
acetic acid
1) THF - diethyl ether, -50 deg C, 1 h, 2) RT, 3 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Arase; Hoshi; Masuda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 209 - 213
反应条件
Yield given. Multistep reaction;
参考文献
Suzuki, Noriyuki; Kondakov, Denis Y.; Kageyama, Motohiro; Kotora, Martin; Hara, Ryuichiro; Takahashi, Tamotsu
Tetrahedron, 1995 , vol. 51, # 15 p. 4519 - 4540
参考文献
Paul; Tchelitcheff
Bulletin de la Societe Chimique de France, 1948 , p. 1200
