1,3-二苯基-1,1,3,3-四甲基二硅氧合成路线 （共 106 条）
反应条件
1: dimethylphenylsilane With dirhodium tetraacetate; potassium carbonate in acetonitrile Schlenk techniqueInert atmosphere; 2: carbon dioxide in acetonitrile T=50°C; P=760.051 Torr; 2 h; Schlenk technique; Reagent/catalystSolvent;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 366, p. 347 - 352
反应条件
1: dimethylphenylsilane With palladium diacetate; potassium carbonate in acetonitrile Schlenk techniqueInert atmosphere; 2: carbon dioxide in acetonitrile T=50°C; 2 h; Schlenk technique; Reagent/catalyst;
参考文献
Itagaki, Shintaro; Yamaguchi, Kazuya; Mizuno, Noritaka
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 366, p. 347 - 352
反应条件
palladium on activated charcoal; hydrogen in THF-d8 (tetrahydrofuran-d8) T=20°C; P=760.051 Torr; 1.5 h;
参考文献
Igarashi, Masayasu; Matsumoto, Tomohiro; Sato, Kazuhiko; Ando, Wataru; Shimada, Shigeru
Chemistry Letters, 2014 , vol. 43, # 4 p. 429 - 431
反应条件
water; sodium hydrogencarbonate in acetone T=0°C; 1 h;
参考文献
Fleming, Ian; Roberts, Richard S.; Smith, Stephen C.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 7 p. 1209 - 1214
反应条件
indium tribromide; oxygen in tetrahydrofuran T=20°C; 2 h;
参考文献
Liu, Ting; Yang, Fan; Li, Yongfeng; Ren, Liang; Zhang, Liqiang; Xu, Kai; Wang, Xian; Xu, Chunming; Gao, Jinsen
Journal of Materials Chemistry A, 2014 , vol. 2, # 1 p. 245 - 250
反应条件
palladium on activated charcoal; hydrogen in THF-d8 (tetrahydrofuran-d8) T=20°C; P=760.051 Torr; 1.5 h; Time;
参考文献
Chemistry Letters, , vol. 43, # 4 p. 429 - 431
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 811,813; engl.Ausg.S.829,831
反应条件
triethyloxonium tetra-fluoroborate; potassium carbonate in acetonitrile T=100°C; 1.5 h; Inert atmosphere;
参考文献
Jorapur, Yogesh R.; Shimada, Toyoshi
Synlett, 2012 , vol. 23, # 11 p. 1633 - 1638
反应条件
1: (RS)-3-hydroxybut-1-yne With n-butyllithium in tetrahydrofuran; hexane T=0°C; 0.5 h; 2: dimethyl(phenyl)silyl chloride in tetrahydrofuran; hexane T=0°C; 2 h; Further stages.;
参考文献
Journal of the American Chemical Society, , vol. 129, # 42 p. 12650 - 12651
反应条件
1 Au/Al2O3; water in ethyl acetate T=25°C; 0.5 h; Reagent/catalyst;
参考文献
Gryparis, Charis; Stratakis, Manolis
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 87 p. 10751 - 10753,3
