1,3-二苯基-1,1,3,3-四甲基二硅氧合成路线 （共 106 条）
反应条件
iron(III) chloride T=140°C;
参考文献
Journal of Organic Chemistry, , vol. 26, p. 2464 - 2467
反应条件
titanium tetrachloride in dichloromethane T=-78 - 22°C;
参考文献
Tetrahedron, , vol. 52, # 3 p. 861 - 868
反应条件
1: 92 percent / (Me3Si)2NH / CH2Cl2 / Ambient temperature 2: 59 percent / tetrahydrofuran / 1.5 h / -78 °C 3: 1.) NaH, 2.) Et3N / 1.) THF, reflux, 3 h, 2.) THF, 15 min View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 7 p. 1215 - 1228
反应条件
(η5-C5H5)Fe(CO)2Me Irradiation;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 38 p. 7052 - 7054
Angewandte Chemie, , vol. 121, # 38 p. 7186 - 7188
反应条件
oxygen in tetrahydrofuran T=0°C; 0.0166667 h; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 7 p. 1209 - 1214
反应条件
1: 98 percent / 1 M HCl / acetone / 1.17 h / 20 °C 2: 4 h / 25 °C / plant cell suspension culture of Symphytum officinale L., pH 5.6 View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 458, # 1-2 p. 13 - 18
反应条件
1: 79 percent / tetrahydrofuran / -78 °C 2: 67 percent / aq. HF / acetonitrile View Scheme
参考文献
Tetrahedron Letters, , vol. 32, # 51 p. 7513 - 7516
反应条件
tris(pentafluorophenyl)-borane in dichloromethane T=0 - 20°C; 0.5 h; Inert atmosphereSchlenk technique; Mechanism;
参考文献
Strasak, Tomas; Sykora, Jan; Lamac, Martin; Kubista, Jiri; Horacek, Michal; Gyepes, Robert; Pinkas, Jiri
Organometallics, 2013 , vol. 32, # 15 p. 4122 - 4129
反应条件
ammonia; water in acetone T=20 - 30°C; Hydrolysis; cocondensation; Further byproducts given;
参考文献
Russian Chemical Bulletin, , vol. 46, # 4 p. 719 - 725
反应条件
tris(acetonitrile)(η5-2,4-cyclopentadien-1-yl)ruthenium(1+) hexafluorophosphate(1-); water in hexadeuterioacetone T=20°C; 24 h; Schlenk technique;
参考文献
Organometallics, , vol. 32, # 16 p. 4457 - 4464
