1,3-二苯基-1,1,3,3-四甲基二硅氧合成路线 （共 106 条）
反应条件
tetra-n-butylammonium tetrafluoroborate; copper(l) chloride in ethylene glycol dimethyl ether electrochemical reaction;
参考文献
Kunai, Atsutaka; Kawakami, Toshihiro; Toyoda, Eiji; Sakurai, Tomohiro; Ishikawa, Mitsuo
Chemistry Letters, 1993 , # 11 p. 1945 - 1948
反应条件
tetra-n-butylammonium perchlorate; copper dichloride in ethylene glycol dimethyl ether electrochemical reaction;
参考文献
Kunai, Atsutaka; Kawakami, Toshihiro; Toyoda, Eiji; Sakurai, Tomohiro; Ishikawa, Mitsuo
Chemistry Letters, 1993 , # 11 p. 1945 - 1948
反应条件
air T=25°C; 4 h; plant cell suspension culture of Symphytum officinale L., pH 5.6; Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 458, # 1-2 p. 13 - 18
反应条件
in cyclohexane 1 h; Ambient temperatureIrradiation;
参考文献
Journal of Organometallic Chemistry, , vol. 412, # 1.2 p. 9 - 19
反应条件
1: 86 percent / pyridine / 4 °C 2: 46 percent / Me2PhSiLi / tetrahydrofuran / 12 h 3: 1.) NaH, 2.) Et3N / 1.) THF, reflux, 3 h, 2.) THF, 15 min View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 7 p. 1215 - 1228
反应条件
1: 63 percent / Na, (CH3)3SiCl / diethyl ether / Heating 2: 86 percent / pyridine / 4 °C 3: 46 percent / Me2PhSiLi / tetrahydrofuran / 12 h 4: 1.) NaH, 2.) Et3N / 1.) THF, reflux, 3 h, 2.) THF, 15 min View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 7 p. 1215 - 1228
反应条件
1: 92 percent / Me2PhSiLi / tetrahydrofuran / 1.) -78 deg C, 2 h, 2.) 0 deg C, 6 h 2: 1.) NaH, 2.) Et3N / 1.) THF, reflux, 3 h, 2.) THF, 15 min View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 7 p. 1215 - 1228
反应条件
1: 59 percent / tetrahydrofuran / 1.5 h / -78 °C 2: 1.) NaH, 2.) Et3N / 1.) THF, reflux, 3 h, 2.) THF, 15 min View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 7 p. 1215 - 1228
反应条件
1: 46 percent / Me2PhSiLi / tetrahydrofuran / 12 h 2: 1.) NaH, 2.) Et3N / 1.) THF, reflux, 3 h, 2.) THF, 15 min View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 7 p. 1215 - 1228
反应条件
in cyclohexane Irradiation (UV/VIS); irradiation of catenate in cyclohexane containing a large excess of 2,3-dimethylbutadiene as trapping agent with a 110 W low pressure Hg arc lamp at room temp. under Ar for 1-4 h; identification by GC and GC-MS;
参考文献
Journal of Organometallic Chemistry, , vol. 412, # 1.2 p. 9 - 19
