1,3-二苯基-1,1,3,3-四甲基二硅氧合成路线 （共 106 条）
反应条件
boron trifluoride in 1,4-dioxane T=30°C; Rate constant;
参考文献
Ruehlmann, K.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 27, p. 139 - 152
反应条件
tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; silver(l) oxide in tetrahydrofuran T=70°C; Hiyama-type coupling; 1 h;
参考文献
Napier, Spencer; Marcuccio, Sebastian M.; Tye, Heather; Whittaker, Mark
Tetrahedron Letters, 2008 , vol. 49, # 24 p. 3939 - 3942
反应条件
tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; silver(l) oxide in tetrahydrofuran; 1,4-dioxane T=70°C; Hiyama-type coupling; 1 h;
参考文献
Napier, Spencer; Marcuccio, Sebastian M.; Tye, Heather; Whittaker, Mark
Tetrahedron Letters, 2008 , vol. 49, # 24 p. 3939 - 3942
反应条件
1: tetrahydrofuran; various solvent(s) / 6 h / 0 °C 2: 10 percent Spectr. / tetrahydrofuran / 192 h / 4 °C View Scheme
参考文献
Fleming, Ian; Roberts, Richard S.; Smith, Stephen C.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 7 p. 1209 - 1214
反应条件
tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; silver(l) oxide in tetrahydrofuran T=70°C; Hiyama-type coupling; 0.5 h;
参考文献
Napier, Spencer; Marcuccio, Sebastian M.; Tye, Heather; Whittaker, Mark
Tetrahedron Letters, 2008 , vol. 49, # 24 p. 3939 - 3942
反应条件
tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; silver(l) oxide in tetrahydrofuran; 1,4-dioxane T=70°C; Hiyama-type coupling; 1 h;
参考文献
Napier, Spencer; Marcuccio, Sebastian M.; Tye, Heather; Whittaker, Mark
Tetrahedron Letters, 2008 , vol. 49, # 24 p. 3939 - 3942
反应条件
sodium hydroxide in methanol; isopropyl alcohol
参考文献
Hyde, J. F.; Johannson, O. K.; Daudt, W. H.; Fleming, R. F.; Laudenslager, H. B.; Roche, M. P.
Journal of the American Chemical Society, 1953 , vol. 75, p. 5615 - 5618
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Gmelin Handbook: Si: MVol.C, 89, page 242 - 246
反应条件
sodium hydroxide in methanol; isopropyl alcohol T=50 - 120°C;
参考文献
Fleming, Ian; Roberts, Richard S.; Smith, Stephen C.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 7 p. 1209 - 1214
反应条件
in 1,4-dioxane; hydrogenchloride T=30°C; Rate constant;
参考文献
Eaborn, C.
Journal of the Chemical Society, 1953 , p. 494 - 501
反应条件
tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; silver(l) oxide in tetrahydrofuran T=70°C; Hiyama-type coupling; 1 h;
参考文献
Napier, Spencer; Marcuccio, Sebastian M.; Tye, Heather; Whittaker, Mark
Tetrahedron Letters, 2008 , vol. 49, # 24 p. 3939 - 3942
