反应条件
BH3*THF in diethylene glycol dimethyl ether CO-atmosphere; addn. of Bu4NCl and BH3*THF to Re-compd., bubbling CO at 110°C for 10 h, cooling to 50°C, Et4NCl addn, stirring for1-2 h; collection (filtration), drying, EtOH addn., stirring for 2 min, collection (filtration), washing (cold EtOH); further crop obtainable from mother liquor by evapn. and treatment with THF;
参考文献
Alberto, Roger; Schibli, Roger; Egli, Andre; Schubiger, P. August; Herrmann, Wolfgang A.; et al.
Journal of Organometallic Chemistry, 1995 , vol. 492, # 2 p. 217 - 224
Title/Abstract Full Text View citing articles Show Details
Alberto, Roger; Schibli, Roger; Egli, Andre; Schubiger, P. August; Herrmann, Wolfgang A.; et al.
Journal of Organometallic Chemistry, 1995 , vol. 493, # 1-2 p. 119 - 128
