反应条件
1: 82 percent / SOCl2 / 1.) room temp., 30 min, 2.) reflux, 90 min; 130 deg C 2: NaBH4 / H2O / 1.5 h / Ambient temperature 3: KOH, Bu4NHSO4 / CHCl3 / 48 h / Irradiation 4: 53 percent / NaI, Bu3SnH, AIBN / 1,2-dimethoxy-ethane / 12 h / Heating 5: 82 percent / Me3SiCl / 2 h / Heating View Scheme
参考文献
Smith, Michael B.; Dembofsky, Bruce T.; Son, Young Chan
Journal of Organic Chemistry, 1994 , vol. 59, # 7 p. 1719 - 1725
