反应条件
1: sodium nitrite; hydrogenchloride / water / 0 - 5 °C / |Inert atmosphere; |Large scale 2: dimethylsulfide borane complex / tetrahydrofuran / 3 h / 20 °C / |Inert atmosphere; |Large scale 3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 5 h / 20 °C / |Reflux; |Inert atmosphere; |Large scale View Scheme
参考文献
Cai, Xiong; Chorghade, Mukund S.; Fura, Aberra; Grewal, Gurmit S.; Jauregui, Karen A.; Lounsbury, Heather A.; Scannell, Ralph T.; Yeh, C. Grace; Young, Michelle A.; Yu, Shaoxia; Guo, Liang; Moriarty, Robert M.; Penmasta, Raju; Rao, Munagala S.; Singhal, Rajesh K.; Song, Zhengzhe; Staszewski, James P.; Tuladhar, Sudersan M.; Yang, Sanmin
Organic Process Research and Development, 1999 , vol. 3, # 1 p. 73 - 76