[2-[2-(2-羟基-乙氧基)-乙氧基]-乙基]-氨基甲酸 9H-芴-9-基甲基酯合成路线 (共 5 条)
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite in dichloromethane Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 133, # 32 p. 12382 - 12385
反应条件
1: pyridine / 18 h / 37 °C
2: pyridine / 18 h / 5 °C
3: NaN3 / dimethylformamide / 5 h / 90 °C
4: aq. ammonia; 2-mercaptoethanol / dimethylformamide / 18 h / 20 °C
5: pyridine / 18 h / 20 °C
6: 440 mg / acetic acid / H2O / 18 h / 20 °C
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参考文献
Khandazhinskaya; Kukhanova; Jasko
Russian Journal of Bioorganic Chemistry, 2005 , vol. 31, # 4 p. 352 - 356
反应条件
1: N,N-dimethyl-formamide / Inert atmosphere
2: hydrazine / ethanol / Inert atmosphere
3: sodium hydrogencarbonate / water / Inert atmosphere
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参考文献
Jalisatgi, Satish S.; Kulkarni, Vikas S.; Tang, Betty; Houston, Zachary H.; Lee, Mark W.; Hawthorne, M. Frederick
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12382 - 12385
反应条件
1: hydrazine / ethanol / Inert atmosphere
2: sodium hydrogencarbonate / water / Inert atmosphere
View Scheme
参考文献
Jalisatgi, Satish S.; Kulkarni, Vikas S.; Tang, Betty; Houston, Zachary H.; Lee, Mark W.; Hawthorne, M. Frederick
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12382 - 12385
反应条件
sodium hydrogencarbonate in water
Inert atmosphere;
参考文献
Jalisatgi, Satish S.; Kulkarni, Vikas S.; Tang, Betty; Houston, Zachary H.; Lee, Mark W.; Hawthorne, M. Frederick
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12382 - 12385