反应条件
1: 87 percent / Thionyl chloride
2: 1.) Triethylamine; 2.) Hydroxybenztriazole, DCC / DMF, room temp., 16 h
3: 63 percent / LiBH4 / 1,2-dimethoxy-ethane / 1.) -78 deg C; 2.) room temp., 2 h
View Scheme
参考文献
Ottenheijm, Harry C.J.; Liskamp, Rob M.J.; Nispen, Simon P.J.M. van; Boots, Hans A.; Tijhuis, Marian W.
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3273 - 3283
