2-[4-(2-甲基-2-丙基)苯基]-1,3-苯并噻唑合成路线 （共 9 条）
反应条件
oxygen; 4-methoxy-2,2,6,6-tetramethylpiperidine-1-oxy in anhydrous xylene
T=100°C; P=760.051 Torr; 3 h;
参考文献
Chen, Yong-Xing; Qian, Ling-Feng; Zhang, Wei; Han, Bing
Angewandte Chemie - International Edition, 2008 , vol. 47, # 48 p. 9330 - 9333
反应条件
1: cyclobenzothiazole With Iron (III) nitrate nonahydrate; dipotassium peroxodisulfate; trifluoroacetic acid in water
T=20°C; 0.166667 h; Schlenk technique;
2: para-tert-butylphenylboronic acid in water
T=70°C; 24 h; Schlenk technique;
参考文献
Deb, Arghya; Manna, Srimanta; Maji, Arun; Dutta, Uttam; Maiti, Debabrata
European Journal of Organic Chemistry, 2013 , # 24 p. 5251 - 5256
反应条件
1-methyl-pyrrolidin-2-one
T=100°C; Jacobson's cyclization; 4 h;
参考文献
Chen, Lianqing; Yang, Chuluo; Li, Suyue; Qin, Jingui
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2007 , vol. 68, # 2 p. 317 - 322
反应条件
oxygen; copper diacetate in dimethyl sulfoxide
T=130°C; 17 h; Sealed tube;
参考文献
Song, Qiuling; Feng, Qiang; Zhou, Mingxin
Organic Letters, 2013 , vol. 15, # 23 p. 5990 - 5993
反应条件
palladium 10 on activated carbon in N-dodecane; N,N-dimethyl acetamide
T=120°C; 28 h; Inert atmosphere;
参考文献
Jin, Xukang; Liu, Yuxiao; Lu, Qiongqiong; Yang, Dejun; Sun, Jiangkai; Qin, Shuangshuang; Zhang, Jingwu; Shen, Jiaxuan; Chu, Changhu; Liu, Renhua
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3776 - 3780
反应条件
palladium diacetate; copper (II) acetate monohydrate in 1,4-dioxane; diethylene glycol dimethyl ether
T=120°C; 24 h; sealed vessel;
参考文献
Chen, Ru; Liu, Saiwen; Liu, Xinhua; Yang, Luo; Deng, Guo-Jun
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 22 p. 7675 - 7679
反应条件
iron sulphate heptahydrate; oxygen in diethylene glycol dimethyl ether; water
T=150°C; 20 h; Sealed tube;
参考文献
Liu, Saiwen; Chen, Ru; Guo, Xiangyu; Yang, Huiqiong; Deng, Guojun; Li, Chao-Jun
Green Chemistry, 2012 , vol. 14, # 6 p. 1577 - 1580
反应条件
K2S; N,N,N',N,-tetramethylethylenediamine; copper(I) bromide in 1-methyl-pyrrolidin-2-one
24 h; Sealed tubeHeating;
参考文献
Zhang, Xiaoyun; Zeng, Weilan; Yang, Yuan; Huang, Hui; Liang, Yun
Organic Letters, 2014 , vol. 16, # 3 p. 876 - 879
反应条件
Iron (III) nitrate nonahydrate; oxygen; [(t-Bu)3PH]BF4 in water; dimethyl sulfoxide
T=120°C; 24 h; Sealed tubeGreen chemistry;
参考文献
Khemnar, Ashok B.; Bhanage, Bhalchandra M.
RSC Advances, 2014 , vol. 4, # 18 p. 8939 - 8942
