3-(2-羟基苯基)-1-苯基丙酮合成路线 （共 20 条）
反应条件
1: 38 mg / Heating
2: 25 mg / aluminium chloride, lithium aluminium hydride / diethyl ether / 12 h / 0 °C
3: potassium hydroxide / methanol / 2 h / Ambient temperature
4: 900 mg / aluminium chloride / 96 h
5: aq. hydrochloric acid / ethanol / 3.5 h
View Scheme
参考文献
Bird, T. Geoffrey C.; Brown, Ben R.; Stuart, Ian A.; Tyrrell, William R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1831 - 1846
反应条件
hydrogenchloride in ethanol
3.5 h;
参考文献
Bird, T. Geoffrey C.; Brown, Ben R.; Stuart, Ian A.; Tyrrell, William R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1831 - 1846
反应条件
1: 40 mg / tri-n-butyltin hydride / benzene / 4 h / Heating
2: 0.76 g / aluminium chloride, lithium aluminium hydride / tetrahydrofuran; diethyl ether / 0.33 h / 0 °C
3: 900 mg / aluminium chloride / 96 h
4: aq. hydrochloric acid / ethanol / 3.5 h
View Scheme
参考文献
Bird, T. Geoffrey C.; Brown, Ben R.; Stuart, Ian A.; Tyrrell, William R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1831 - 1846
反应条件
1: 900 mg / aluminium chloride / 96 h
2: aq. hydrochloric acid / ethanol / 3.5 h
View Scheme
参考文献
Bird, T. Geoffrey C.; Brown, Ben R.; Stuart, Ian A.; Tyrrell, William R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1831 - 1846
反应条件
1: potassium hydroxide / methanol / 2 h / Ambient temperature
2: 900 mg / aluminium chloride / 96 h
3: aq. hydrochloric acid / ethanol / 3.5 h
View Scheme
参考文献
Bird, T. Geoffrey C.; Brown, Ben R.; Stuart, Ian A.; Tyrrell, William R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1831 - 1846
反应条件
1: Heating
2: 25 mg / aluminium chloride, lithium aluminium hydride / diethyl ether / 12 h / 0 °C
3: potassium hydroxide / methanol / 2 h / Ambient temperature
4: 900 mg / aluminium chloride / 96 h
5: aq. hydrochloric acid / ethanol / 3.5 h
View Scheme
参考文献
Bird, T. Geoffrey C.; Brown, Ben R.; Stuart, Ian A.; Tyrrell, William R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1831 - 1846
反应条件
1: 25 mg / aluminium chloride, lithium aluminium hydride / diethyl ether / 12 h / 0 °C
2: potassium hydroxide / methanol / 2 h / Ambient temperature
3: 900 mg / aluminium chloride / 96 h
4: aq. hydrochloric acid / ethanol / 3.5 h
View Scheme
参考文献
Bird, T. Geoffrey C.; Brown, Ben R.; Stuart, Ian A.; Tyrrell, William R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1831 - 1846
反应条件
methanol; Pd/SrCO3
Hydrogenation;
参考文献
Aulin-Erdtman et al.
Svensk Papperstidn. 50<1947> Haegglund-Festschr.S.81,84
反应条件
bei der Destillation unter vermindertem Druck;
参考文献
Borsche; Geyer
Chemische Berichte, 1914 , vol. 47, p. 1159
反应条件
dihydrogen peroxide; tetra-(n-butyl)ammonium iodide in water
T=20°C; chemoselective reaction;
参考文献
Uyanik, Muhammet; Okamoto, Hiroaki; Yasui, Takeshi; Ishihara, Kazuaki
Science, 2010 , vol. 328, # 5984 p. 1376 - 1379
