(E)-1-甲氧基-2-己烯合成路线 （共 3 条）
反应条件
zirconocene dichloride 1.) THF, -78 deg C, 1 h, 2.) THF, RT, 6 h; Yield given. Multistep reaction;
参考文献
Suzuki, Noriyuki; Kondakov, Denis Y.; Takahashi, Tamotsu
Journal of the American Chemical Society, 1993 , vol. 115, # 18 p. 8485 - 8486
反应条件
sodium hydride in N,N-dimethyl-formamide; mineral oil
T=20°C; 2 h;
参考文献
Park, Sae Rom; Kim, Cheoljae; Kim, Dong-Gil; Thrimurtulu, Neetipalli; Yeom, Hyun-Suk; Jun, Jungho; Shin, Seunghoon; Rhee, Young Ho
Organic Letters, 2013 , vol. 15, # 6 p. 1166 - 1169
反应条件
1.1: diisobutylaluminium hydride / dichloromethane / -78 °C / |Inert atmosphere
2.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C / |Inert atmosphere
2.2: 16 h / 0 - 20 °C / |Inert atmosphere
View Scheme
参考文献
Perez, Manuel; Fananas-Mastral, Martin; Hornillos, Valentin; Rudolph, Alena; Bos, Pieter H.; Harutyunyan, Syuzanna R.; Feringa, Ben L.
Chemistry - A European Journal, 2012 , vol. 18, # 38 p. 11880 - 11883
