反应条件
1: 86 percent / LAH / diethyl ether / 0.5 h / 0 °C
2: 71 percent / pyridinium chlorochromate (PCC) / CH2Cl2 / 0 °C
3: 1.) magnesium / 1.) THF, RT, 1 h, 2.) RT, 5 min
4: 1.) p-toluenesulfonic acid, 2.) 6 N aq. HCl / 1.) acetone, RT, 3 h, 2.) THF, reflux, 5 h
View Scheme
参考文献
Wilson, Stephen R.; Zucker, Paul A.
Journal of Organic Chemistry, 1988 , vol. 53, # 20 p. 4682 - 4693
