2,2-二甲基-5-己烯-1-醇合成路线 （共 17 条）
反应条件
lithium aluminium tetrahydride in diethyl ether T=-78 - 0°C; 1.33333 h;
参考文献
Thalji, Reema K.; Roush, William R.
Journal of the American Chemical Society, 2005 , vol. 127, # 48 p. 16778 - 16779
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 3 h; 2: With sodium hydroxide; water in tetrahydrofuran T=0°C;
参考文献
Jandeleit, Bernd; Li, Yunxiao; Gallop, Mark A.; Zerangue, Noa; Virsik, Peter A.; Fischer, Wolf-Nicolas
Patent: US2009/69419 A1, 2009 ;
Location in patent: Page/Page column 54 ;
反应条件
1: 3,3-dimethyloxacyclobutane With 4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=0°C; 2 h; 2: allyl bromide in tetrahydrofuran T=0 - 20°C;
参考文献
Hilt, Gerhard; Treutwein, Jonas
Chemical Communications, 2009 , # 11 p. 1395 - 1397
反应条件
1: HCl / 20 h / 0 °C 2: 1) Mg / THF 3: LiAlH4 / diethyl ether / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 19 p. 3545 - 3556
反应条件
1: 1) Mg / THF 2: LiAlH4 / diethyl ether / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 19 p. 3545 - 3556
反应条件
sodium tetrahydroborate in methanol
参考文献
Journal of the American Chemical Society, , vol. 97, p. 2778 - 2785
反应条件
1: pyridinium chlorochromate / CH2Cl2 / 2 h / 25 °C 2: PCl5 / hexane / 24 h / 25 °C 3: 17 percent Chromat. / Mg, DCPH / tetrahydrofuran / 8 h / 25 °C View Scheme
参考文献
Ashby, E. C.; Deshpande, Abhay K.; Doctorovich, Fabio
Journal of Organic Chemistry, 1994 , vol. 59, # 21 p. 6223 - 6232
反应条件
1: 93 percent / triphenylphosphine, I2, pyridine / benzene / 24 h / Heating 2: 60 percent / hexaphenylditin / benzene / 15 h / Heating View Scheme
参考文献
Ashby, E. C.; Park, B.; Patil, G. S.; Gadru, K.; Gurumurthy, R.
Journal of Organic Chemistry, 1993 , vol. 58, p. 424 - 437
反应条件
1: pyridinium chlorochromate / CH2Cl2 / 2 h / 25 °C
2: hydrazine hydrate / ethanol / 1 h / Heating
3: I2, Et3N / diethyl ether
4: 10 percent Chromat. / LiAlH4 / tetrahydrofuran / 21 h / 25 °C
View Scheme
参考文献
Ashby, E. C.; Deshpande, Abhay K.; Doctorovich, Fabio
Journal of Organic Chemistry, 1994 , vol. 59, # 21 p. 6223 - 6232
反应条件
pyridine; iodine; triphenylphosphine in benzene
24 h; Heating;
参考文献
Ashby, E. C.; Park, B.; Patil, G. S.; Gadru, K.; Gurumurthy, R.
Journal of Organic Chemistry, 1993 , vol. 58, p. 424 - 437
