3-(4-乙酰氧基苯基)-2-氧代丙醛合成路线 （共 8 条）
反应条件
hydrogenchloride in ethanol T=80°C; 4.5 h;
参考文献
Keenan, Martine; Jones, Keith; Hibbert, Frank
Chemical Communications, 1997 , # 3 p. 323 - 324
反应条件
1: 10percent aq. HCl / dioxane; H2O / 100 °C 2: DCC / pyridine / Ambient temperature 3: H2 / Pd/C View Scheme
参考文献
Teranishi; Goto
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 11 p. 3132 - 3140
反应条件
sodium acetate; dimethyl sulfoxide
0.416667 h; Ambient temperature;
参考文献
Keenan, Martine; Jones, Keith; Hibbert, Frank
Chemical Communications, 1997 , # 3 p. 323 - 324
反应条件
1: 84 percent / NaOAc / 2 h / Heating
2: SOCl2 / 12 h / Ambient temperature
3: diethyl ether / 1.5 h / 0 °C
4: HBr / 0.5 h / 0 °C
5: 98 percent / AgNO3 / acetonitrile / 12 h
6: 88 percent / NaOAc*3H2O, DMSO / 0.42 h / Ambient temperature
View Scheme
参考文献
Keenan, Martine; Jones, Keith; Hibbert, Frank
Chemical Communications, 1997 , # 3 p. 323 - 324
反应条件
1: 98 percent / AgNO3 / acetonitrile / 12 h
2: 88 percent / NaOAc*3H2O, DMSO / 0.42 h / Ambient temperature
View Scheme
参考文献
Keenan, Martine; Jones, Keith; Hibbert, Frank
Chemical Communications, 1997 , # 3 p. 323 - 324
反应条件
1: HBr / 0.5 h / 0 °C
2: 98 percent / AgNO3 / acetonitrile / 12 h
3: 88 percent / NaOAc*3H2O, DMSO / 0.42 h / Ambient temperature
View Scheme
参考文献
Keenan, Martine; Jones, Keith; Hibbert, Frank
Chemical Communications, 1997 , # 3 p. 323 - 324
反应条件
1: diethyl ether / 1.5 h / 0 °C
2: HBr / 0.5 h / 0 °C
3: 98 percent / AgNO3 / acetonitrile / 12 h
4: 88 percent / NaOAc*3H2O, DMSO / 0.42 h / Ambient temperature
View Scheme
参考文献
Keenan, Martine; Jones, Keith; Hibbert, Frank
Chemical Communications, 1997 , # 3 p. 323 - 324
反应条件
1: SOCl2 / 12 h / Ambient temperature
2: diethyl ether / 1.5 h / 0 °C
3: HBr / 0.5 h / 0 °C
4: 98 percent / AgNO3 / acetonitrile / 12 h
5: 88 percent / NaOAc*3H2O, DMSO / 0.42 h / Ambient temperature
View Scheme
参考文献
Keenan, Martine; Jones, Keith; Hibbert, Frank
Chemical Communications, 1997 , # 3 p. 323 - 324
