3-硝基-4-氯二苯甲酮合成路线 （共 22 条）
反应条件
1: Cl(CO)2Cl, DMF / CH2Cl2 / Ambient temperature 2: AlCl3 / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 62, # 17 p. 5908 - 5919
反应条件
aluminium trichloride T=70 - 85°C;
参考文献
Chemische Berichte, , vol. 47, p. 2782
Chemische Berichte, , vol. 49, p. 2274
反应条件
1: NH3 2: (i) Fe, aq. NH4Cl, (ii) aq. HCl View Scheme
参考文献
Raeymackers; Van Gelder; Roevens; Janssen
Arzneimittel-Forschung/Drug Research, 1978 , vol. 28, # 4 p. 586 - 594
反应条件
ammonium hydroxide in formamide T=120°C; P=3000.2 - 3750.3 Torr; 6 h;
参考文献
Niclas, Hans-Joachim; Bohle, Matthias; Rick, Jens-Detlev; Zeuner, Frank; Zoelch, Lothar
Zeitschrift fuer Chemie (Stuttgart, Germany), 1985 , vol. 25, # 4 p. 137 - 138
反应条件
N-butylamine in water; toluene
参考文献
Rohm and Haas Company
Patent: US4060636 A1, 1977 ;
反应条件
1: 98 percent / methanol / 2 h / Heating
2: 69.2 percent / Zn; AcOH / 12 h
View Scheme
参考文献
El-Hamouly; Abd-Allah; Tawfik
Egyptian Journal of Chemistry, 2004 , vol. 47, # 3 p. 333 - 343
反应条件
hydrogenchloride; methylamine in methanol; dichloromethane
参考文献
Ciba-Geigy Corporation
Patent: US4141982 A1, 1979 ;
反应条件
in methanol
2 h; Heating;
参考文献
El-Hamouly; Abd-Allah; Tawfik
Egyptian Journal of Chemistry, 2004 , vol. 47, # 3 p. 333 - 343
反应条件
1: methanol
2: ethanol
View Scheme
参考文献
van Alphen
Recueil des Travaux Chimiques des Pays-Bas, 1930 , vol. 49, p. 383,387
参考文献
van Alphen
Recueil des Travaux Chimiques des Pays-Bas, 1930 , vol. 49, p. 383,387
