3-(4-叔丁基苯基)-2-甲基丙醇合成路线 (共 6 条)
反应条件
hydrogen
T=200 - 240°C; P=37503.8 - 105011 Torr; 200 - 3100 h; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2009/82562 A1, 2009 ;
Location in patent: Page/Page column 7-8 ;
反应条件
sodium tetrahydroborate in methanol
T=0 - 20°C; 2 h;
参考文献
Rosini, Goffredo; Paolucci, Claudio; Boschi, Francesca; Marotta, Emanuela; Righi, Paolo; Tozzi, Francesco
Green Chemistry, 2010 , vol. 12, # 10 p. 1747 - 1757
反应条件
5 Pd(II)/C(eggshell); hydrogen in methanol
T=39.84°C; P=3750.38 Torr; 0.1 h; Autoclave;
参考文献
Du, Wen Qiang; Rong, Ze Ming; Liang, Yan; Wang, Yong; Lu, Xin Yi; Wang, Yi Fan; Lu, Lian Hai
Chinese Chemical Letters, 2012 , vol. 23, # 7 p. 773 - 776
反应条件
AlCl3, aluminium chloride in dichloromethane
T=1 - 10°C; Friedel Crafts Alkylation; 4 h; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2012/209030 A1, 2012 ;
Location in patent: Page/Page column 4-5 ;
反应条件
hydrogen; silica gel; nickel in ethanol; water
T=99.9°C; P=15001.2 Torr; influence of different temperatures; selectivity of the reaction; Product distribution;
参考文献
Pak; Konuspaev; Sagindykov; Sokol'skii; Zapletal; Prykhlik
Journal of applied chemistry of the USSR, 1986 , vol. 59, # 5 pt 2 p. 1058 - 1060
参考文献
Hoffmann-La Roche Inc.
Patent: US4241058 A1, 1980 ;