N,N′,N′′-三(对甲苯磺酰)二乙撑三胺合成路线 （共 18 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=30°C; 24 h;
参考文献
Chavez, F.; Sherry, A. D.
Journal of Organic Chemistry, 1989 , vol. 54, # 12 p. 2990 - 2992
反应条件
sodium hydride in various solvents; N,N-dimethyl-formamide T=105°C; 8 h;
参考文献
Gao, Jinzhang; He, Hui; Zhang, Xuan; Lu, Xiaoquan; Kang, Jingwan
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 2 p. 372 - 375
反应条件
sodium methylate
1.) MeOH; 2.) DMF, a.) 110 deg C, 3 h; b.) 130 deg C, 15 min; c.) RT, 14 h; Yield given. Multistep reaction;
参考文献
Pilichowski, J. F.; Lehn, J. M.; Sauvage, J. P.; Gramain, J. C.
Tetrahedron, 1985 , vol. 41, # 10 p. 1959 - 1964
反应条件
hydrogen bromide; sodium; acetic acid; phenol
Yield given. Multistep reaction;
参考文献
Comarmond,J.; Plumere,P.; Lehn,J.M.
Journal of the American Chemical Society, 1982 , vol. 104, p. 6330
反应条件
hydrogen bromide; sodium; acetic acid; phenol
Yield given. Multistep reaction;
参考文献
Comarmond,J.; Plumere,P.; Lehn,J.M.
Journal of the American Chemical Society, 1982 , vol. 104, p. 6330
反应条件
ethanol; sodium
Heating / reflux;
参考文献
Hasserodt, Jens
Patent: US2007/218010 A1, 2007 ;
Location in patent: Page/Page column 19 ;
反应条件
sodium hydride in various solvents; N,N-dimethyl-formamide
T=105°C; 8 h;
参考文献
Gao, Jinzhang; He, Hui; Zhang, Xuan; Lu, Xiaoquan; Kang, Jingwan
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 2 p. 372 - 375
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=30°C; 72 h;
参考文献
Chavez, F.; Sherry, A. D.
Journal of Organic Chemistry, 1989 , vol. 54, # 12 p. 2990 - 2992
