DL-苯基丙氨酸甲酯盐酸盐合成路线 （共 39 条）
反应条件
thionyl chloride in methanol T=20°C;
参考文献
Guo, Xiaoke; Yang, Qian; Xu, Jing; Zhang, Li; Chu, Hongxi; Yu, Peng; Zhu, Yingying; Wei, Jinglian; Chen, Weilin; Zhang, Yaozhong; Zhang, Xiaojin; Sun, Haopeng; Tang, Yiqun; You, Qidong
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 21 p. 6466 - 6476
反应条件
thionyl chloride T=5 - 50°C; 25 h;
参考文献
Kaptein, Bernard; Noorduin, Wim L.; Meekes, Hugo; Van Enckevort, Willem J. P.; Kellogg, Richard M.; Vlieg, Elias
Angewandte Chemie - International Edition, 2008 , vol. 47, # 38 p. 7226 - 7229
反应条件
hydrogen; palladium on activated charcoal in methanol 6 h; Ambient temperature;
参考文献
Portelli, Mario
Gazzetta Chimica Italiana, 1989 , vol. 119, # 4 p. 215 - 216
反应条件
formic acid; palladium in methanol 2 h; Ambient temperature;
参考文献
Gray, Brian D.; Jeffs, Peter W.
Journal of the Chemical Society, Chemical Communications, 1987 , # 18 p. 1329 - 1330
反应条件
hydrogenchloride in water 1 h; Reflux;
参考文献
Tetrahedron, , vol. 70, # 13 p. 2264 - 2271
反应条件
hydrogenchloride in methanol electrolysis;
参考文献
Khalifa, M. Hassen; Rieker, Anton
Tetrahedron Letters, 1984 , vol. 25, # 10 p. 1027 - 1030
反应条件
1: SOCl2 / 4 h 2: SOCl2 / 10 h / Heating 3: 87 percent / H2 / 10percent Pd/C / methanol / 6 h / Ambient temperature View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 119, # 4 p. 215 - 216
反应条件
1: 74.8 percent / NaOH / methanol; H2O / 1.) 16 dg C, 30 min; 2.) RT, overnight 2: SOCl2 / 4 h 3: SOCl2 / 10 h / Heating 4: 87 percent / H2 / 10percent Pd/C / methanol / 6 h / Ambient temperature View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 119, # 4 p. 215 - 216
反应条件
1: SOCl2 / 10 h / Heating 2: 87 percent / H2 / 10percent Pd/C / methanol / 6 h / Ambient temperature View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 119, # 4 p. 215 - 216
反应条件
1: hydrogenchloride; water / 30 h / |Reflux 2: hydrogenchloride / water / 1 h / |Reflux View Scheme
参考文献
Tetrahedron, , vol. 70, # 13 p. 2264 - 2271
