4,4-二甲基-1,3-环己二酮合成路线 （共 13 条）
反应条件
sodium methylate in diethyl ether T=5 - 20°C;
参考文献
Wyeth
Patent: US2006/14826 A1, 2006 ;
Location in patent: Page/Page column 14 ;
反应条件
potassium tert-butylate in tetrahydrofuran T=25°C; Michael addition-Claisen condensation; 0.5 h;
参考文献
Ishikawa, Teruhiko; Kadoya, Ryuichiro; Arai, Masaki; Takahashi, Haruka; Kaisi, Yumi; Mizuta, Tomohiro; Yoshikai, Kazusa; Saito, Seiki
Journal of Organic Chemistry, 2001 , vol. 66, # 24 p. 8000 - 8009
反应条件
potassium tert-butylate in tetrahydrofuran T=25°C; Michael addition-Claisen condensation; 0.5 h;
参考文献
Ishikawa, Teruhiko; Kadoya, Ryuichiro; Arai, Masaki; Takahashi, Haruka; Kaisi, Yumi; Mizuta, Tomohiro; Yoshikai, Kazusa; Saito, Seiki
Journal of Organic Chemistry, 2001 , vol. 66, # 24 p. 8000 - 8009
反应条件
potassium tert-butylate in tetrahydrofuran; tert-butyl alcohol T=20°C; 12 h; Further byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 66, # 24 p. 8000 - 8009
反应条件
sodium methylate in benzene
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 2, p. 1771 - 1773
Zhurnal Organicheskoi Khimii, , vol. 2, p. 1801 - 1804
反应条件
1: Heating 2: SOCl2 3: (i) Mg, Et2O, (ii) CdCl2, (iii) /BRN= 1770995/, benzene 4: NaOMe / diethyl ether View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 42, p. 212 - 222
反应条件
1: SOCl2 2: (i) Mg, Et2O, (ii) CdCl2, (iii) /BRN= 1770995/, benzene 3: NaOMe / diethyl ether View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 42, p. 212 - 222
反应条件
1: (i) Mg, Et2O, (ii) CdCl2, (iii) /BRN= 1770995/, benzene 2: NaOMe / diethyl ether View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 42, p. 212 - 222
反应条件
potassium tert-butylate
参考文献
Journal of the Indian Chemical Society, , vol. 36, p. 299
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 1, p. 1018 - 1023
Zhurnal Organicheskoi Khimii, , vol. 1, # 6 p. 1010 - 1016
