(E)-11-十六碳烯-1-醇乙酸酯合成路线 （共 36 条）
反应条件
sodium hydroxide in ethanol 0.5 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 51, # 26 p. 5282 - 5286
参考文献
Zarbin, Paulo H. G.; Lorini, Lisete M.; Ambrogi, Bianca G.; Vidal, Diogo M.; Lima, Eraldo R.
Journal of Chemical Ecology, 2007 , vol. 33, # 3 p. 555 - 565
反应条件
potassium iodide in acetic acid
24 h; Heating;
参考文献
Zakharkin, L. I.; Petrushkina, E. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 8 p. 1419 - 1422
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 8 p. 1623 - 1628
反应条件
in acetic acid
T=35 - 40°C;
参考文献
Vig, O. P.; Sharma, M. L.; Vohra, Neelam; Sabharwal, Arun; Huq, M. A.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 1069 - 1070
反应条件
in acetonitrile
0.5 h; Ambient temperature;
参考文献
Soderquist, John A.; Anderson, Charles L.
Tetrahedron Letters, 1988 , vol. 29, # 23 p. 2777 - 2778
反应条件
1: PBr3, pyridine
2: 1.) Mg / 2.) Li2CuCl4 / 1.) THF; 2.) 0 deg C, 3 h, 20 deg C, 1 h
3: 89 percent / potassium iodide / acetic acid / 24 h / Heating
View Scheme
参考文献
Zakharkin, L. I.; Petrushkina, E. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 8 p. 1419 - 1422
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 8 p. 1623 - 1628
反应条件
1: 1.) Mg / 2.) Li2CuCl4 / 1.) THF; 2.) 0 deg C, 3 h, 20 deg C, 1 h
2: 89 percent / potassium iodide / acetic acid / 24 h / Heating
View Scheme
参考文献
Zakharkin, L. I.; Petrushkina, E. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 8 p. 1419 - 1422
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 8 p. 1623 - 1628
反应条件
1: 1.) Mg / 2.) Li2CuCl4 / 1.) THF; 2.) 0 deg C, 3 h, 20 deg C, 1 h
2: 89 percent / potassium iodide / acetic acid / 24 h / Heating
View Scheme
参考文献
Zakharkin, L. I.; Petrushkina, E. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 8 p. 1419 - 1422
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 8 p. 1623 - 1628
反应条件
1: PBr3 / 1.) pyridine, hexane, 3-5 deg C, 3h; 2.) 20 deg C, 12 h
2: 1.) Mg / 2.) Li2CuCl4 / 1.) THF; 2.) 0 deg C, 3 h, 20 deg C, 1 h
3: 89 percent / potassium iodide / acetic acid / 24 h / Heating
View Scheme
参考文献
Zakharkin, L. I.; Petrushkina, E. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 8 p. 1419 - 1422
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 8 p. 1623 - 1628
反应条件
1: 1.) 0.75M 9-borabicyclo<3.3.1>nonane; 2.) 3N NaOH, 26percent H2O2 / 1.) THF, 0 deg C, 2-3 h; 2.) 20 deg C, 2-3 h
2: PBr3 / 1.) pyridine, hexane, 3-5 deg C, 3h; 2.) 20 deg C, 12 h
3: 1.) Mg / 2.) Li2CuCl4 / 1.) THF; 2.) 0 deg C, 3 h, 20 deg C, 1 h
4: 89 percent / potassium iodide / acetic acid / 24 h / Heating
View Scheme
参考文献
Zakharkin, L. I.; Petrushkina, E. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 8 p. 1419 - 1422
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 8 p. 1623 - 1628
