(E)-11-十六碳烯-1-醇乙酸酯合成路线 （共 36 条）
反应条件
1: 52 percent / Li2CuCl4 / tetrahydrofuran / 4 h / -10 °C
2: 68 percent / acetic acid / 35 - 40 °C
View Scheme
参考文献
Vig, O. P.; Sharma, M. L.; Vohra, Neelam; Sabharwal, Arun; Huq, M. A.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 1069 - 1070
反应条件
K(iPrO)3BH; thexylchloroborane*methyl sulfide; sodium methylate; acetic acid
Yield given. Multistep reaction;
参考文献
Brown, Herbert C.; Lee, Hsiupu D.; Kulkarni, Surendra U.
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5282 - 5286
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane)
1.) ether, 12 h, room temp., 2.) 80 deg C, 15 h; Yield given. Multistep reaction;
参考文献
Fiandanese, Vito; Marchese, Giuseppe; Naso, Francesco; Ronzini, Ludovico
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1115 - 1120
反应条件
pyridine
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane)
1.) ether, 12 h, room temp., 2.) 80 deg C, 15 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Fiandanese, Vito; Marchese, Giuseppe; Naso, Francesco; Ronzini, Ludovico
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1115 - 1120
反应条件
1: 97 percent / 20percent aq. NaOH / aq. ethanol / 0.5 h / Ambient temperature
2: 98 percent / oxalyl chloride, Me2SO / CH2Cl2 / 0.25 h / -60 °C
View Scheme
参考文献
Brown, Herbert C.; Lee, Hsiupu D.; Kulkarni, Surendra U.
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5282 - 5286
