Α-羟基-Α-甲苄基甲苯酮合成路线 （共 41 条）
反应条件
Pd2hpp4; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; oxygen in tetrahydrofuran T=6°C; P=760.051 Torr; 12 h; regioselective reaction;
参考文献
Chuang, Gary Jing; Wang, Weike; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 6 p. 1760 - 1762
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=30°C; 0.5 h;
参考文献
Moorthy, Jarugu Narasimha; Singhal, Nidhi; Senapati, Kalyan
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 5 p. 767 - 771
反应条件
sodium hydroxide in dimethyl sulfoxide
参考文献
Justus Liebigs Annalen der Chemie, , vol. 735, p. 56 - 64
反应条件
1: With chloro-trimethyl-silane; (EtCp)2TiCl2; triethyl amine hydrochloride; zinc in tetrahydrofuran T=35°C; 48 h; Schlenk techniqueInert atmosphereSealed tube; 2: With tetrabutyl ammonium fluoride in tetrahydrofuran 1 h; Schlenk techniqueInert atmosphere; 3: With water in tetrahydrofuran 0.0833333 h; Schlenk techniqueInert atmosphere;
参考文献
Feurer, Markus; Frey, Georg; Luu, Hieu-Trinh; Kratzert, Daniel; Streuff, Jan
Chemical Communications, 2014 , vol. 50, # 40 p. 5370 - 5372
反应条件
in tetrahydrofuran; diethyl ether T=-78°C; 1.5 h;
参考文献
Fleming, Ian; Roberts, Richard S.; Smith, Stephen C.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 7 p. 1215 - 1228
反应条件
samarium diiodide in tetrahydrofuran 10 h; Heating;
参考文献
Tetrahedron Letters, , vol. 39, # 46 p. 8491 - 8494
反应条件
samarium diiodide in tetrahydrofuran 9 h; Heating;
参考文献
Tetrahedron Letters, , vol. 42, # 33 p. 5745 - 5748
反应条件
sodium amalgam; diethyl ether; benzene anschliessendes Behandeln mit Methyljodid;
参考文献
Journal of the American Chemical Society, , vol. 56, p. 963
反应条件
samarium diiodide; benzonitrile in tetrahydrofuran 10 h; Heating;
参考文献
Tetrahedron Letters, , vol. 39, # 46 p. 8491 - 8494
反应条件
[Rh(NCMe)2(cod)][BF4] in tetrahydrofuran T=60°C; 20 h; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 59, # 24 p. 4351 - 4361
