1-硫代-Β-D-乙基半乳糖苷合成路线 （共 4 条）
反应条件
methanol; sodium methylate 20 h; Ambient temperature;
参考文献
Weiwer, Michel; Sherwood, Trevor; Linhardt, Robert J.
Journal of Carbohydrate Chemistry, 2008 , vol. 27, # 7 p. 420 - 427
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane T=0°C; 6 h; 2: With sodium methylate in methanol T=20°C; Zemplen deacetylation; 20 h;
参考文献
Khaja, Sirajud D.; Kumar, Vipin; Ahmad, Misbah; Xue, Jun; Matta, Khushi L.
Tetrahedron Letters, 2010 , vol. 51, # 33 p. 4411 - 4414
反应条件
1: 98 percent / boron trifluoride diethyl etherate / CH2Cl2 / 3 h / 20 °C 2: NaOMe / methanol / 1 h / 20 °C View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 19, # 7 p. 891 - 921
参考文献
Journal of the American Chemical Society, , vol. 71, p. 140,142
