methanol; sodium hydroxide; Dicyanonaphthalene 10 h; Irradiation;

C22H26Cl2NPPd; sodium t-butanolate in toluene T=110°C; 22 h; Inert atmosphere;

thallium(III) nitrate Ambient temperature;

sodium tetrahydroborate; tin(IV) chloride 1.) CH2Cl2, 2.) MeOH; Yield given. Multistep reaction. Yields of byproduct given;

methanol; sodium hydroxide; Dicyanonaphthalene 10 h; Irradiation;

1: 72 percent / thallium(III) nitrate / acetonitrile 2: 1.) cerium(IV) ammonium nitrate, 2.) conc. H2SO4, urea / 1.) acetic acid, room temperature, 2.) 80 deg C, 20 h 3: chromium trioxide / acetic acid / 48 h / Ambient temperature View Scheme