(3,4,5,6-四氢-4-甲基-3-氧代吡嗪基)-氰胺合成路线 （共 3 条）
反应条件
in ethanol
T=58 - 60°C; 4 h;
参考文献
Samaritoni, Jack G.; Demeter, David A.; Gifford, James M.; Watson, Gerald B.; Kempe, Margaret S.; Bruce, Timothy J.
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 10 p. 3035 - 3042
反应条件
1: 83 percent / Lawesson's reagent / toluene / 1.5 h / 45 - 50 °C
2: 64 percent / K2CO3 / acetonitrile / 0 - 20 °C
3: 47 percent / ethanol / 4 h / 58 - 60 °C
View Scheme
参考文献
Samaritoni, Jack G.; Demeter, David A.; Gifford, James M.; Watson, Gerald B.; Kempe, Margaret S.; Bruce, Timothy J.
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 10 p. 3035 - 3042
反应条件
1: 64 percent / K2CO3 / acetonitrile / 0 - 20 °C
2: 47 percent / ethanol / 4 h / 58 - 60 °C
View Scheme
参考文献
Samaritoni, Jack G.; Demeter, David A.; Gifford, James M.; Watson, Gerald B.; Kempe, Margaret S.; Bruce, Timothy J.
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 10 p. 3035 - 3042
