(3,4,5,6-四氢-4-甲基-5-氧代吡嗪基)-氰胺合成路线 （共 3 条）
反应条件
in ethanol
T=60 - 70°C; 3 h;
参考文献
Samaritoni, Jack G.; Demeter, David A.; Gifford, James M.; Watson, Gerald B.; Kempe, Margaret S.; Bruce, Timothy J.
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 10 p. 3035 - 3042
反应条件
1.1: Lawesson's reagent / toluene / 1 h / 55 - 60 °C
1.2: 1.5 g / K2CO3 / acetonitrile / 20 °C
2.1: 52 percent / ethanol / 3 h / 60 - 70 °C
View Scheme
参考文献
Samaritoni, Jack G.; Demeter, David A.; Gifford, James M.; Watson, Gerald B.; Kempe, Margaret S.; Bruce, Timothy J.
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 10 p. 3035 - 3042
反应条件
1.1: 82 percent / ethane-1,2-diol / 0.67 h / Heating
2.1: Lawesson's reagent / toluene / 1 h / 55 - 60 °C
2.2: 1.5 g / K2CO3 / acetonitrile / 20 °C
3.1: 52 percent / ethanol / 3 h / 60 - 70 °C
View Scheme
参考文献
Samaritoni, Jack G.; Demeter, David A.; Gifford, James M.; Watson, Gerald B.; Kempe, Margaret S.; Bruce, Timothy J.
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 10 p. 3035 - 3042
