3,6-二噁-8-疏基辛烷-1-醇合成路线 (共 6 条)
反应条件
sodium hydrogensulfide in ethanol
Substitution;
参考文献
Boden, Neville; Bushby, Richard J.; Liu, Quanying; Evans, Stephen D.; Toby; Jenkins; Knowles, Peter F.; Miles, Robert E.
Tetrahedron, 1998 , vol. 54, # 38 p. 11537 - 11548
反应条件
sodium hydrogensulfide in methanol
3 h; Ambient temperature;
参考文献
Asseline; Bonfils; Kurfurst; Chassignol; Roig; Thuong
Tetrahedron, 1992 , vol. 48, # 7 p. 1233 - 1254
反应条件
hydrogenchloride; sodium hydroxide; thiourea in deoxygenated H2O; water
参考文献
Hutchison, James E.; Woehrle, Gerd H.; Warner, Marvin G.; Brown, Leif O.
Patent: US2009/99044 A1, 2009 ;
反应条件
1: With sodium methylate in methanol
T=20°C; 14 h; Inert atmosphere;
2:
参考文献
Conte, Mauro Lo; Robb, Maxwell J.; Hed, Yvonne; Marra, Alberto; Malkoch, Michael; Hawker, Craig J.; Dondoni, Alessandro
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 20 p. 4468 - 4475
反应条件
1: in water
2 h; Heating;
2: With sodium hydroxide
2 h; Heating;
参考文献
Charvet, Nicolas; Reiss, Peter; Roget, Andre; Dapuis, Alain; Gruenwald, Didier; Carayon, Sophie; Chandezon, Frederic; Livache, Thierry
Journal of Materials Chemistry, 2004 , vol. 14, # 17 p. 2638 - 2642
反应条件
ammonium hydroxide; oxygen
48 h; pH 8;
参考文献
Asseline; Bonfils; Kurfurst; Chassignol; Roig; Thuong
Tetrahedron, 1992 , vol. 48, # 7 p. 1233 - 1254