2-甲氧基-5-(三氟甲氧基)苄醇合成路线 (共 2 条)
反应条件
sodium tetrahydroborate in methanol T=20°C;
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/821 A1, 2005 ;
Location in patent: Page 49 ;
WO 2005/000821 A1
反应条件
1: With thionyl chloride in DMF (N,N-dimethyl-formamide)
T=20°C; 1 h;
2: With potassium carbonate
1 h;
3: With sodium azide in dimethyl sulfoxide
T=20°C;
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/821 A1, 2005 ;
Location in patent: Page 50 ;
WO 2005/000821 A1