5,6-二溴-1,10-菲罗啉合成路线 （共 7 条）
反应条件
sulfuric acid, fuming; bromine
T=150°C; 60 h;
参考文献
Chesneau, Bertrand; Passelande, Angelique; Hudhomme, Pietrick
Organic Letters, 2009 , vol. 11, # 3 p. 649 - 652
反应条件
1: H2SO4
2: arsenic acid; concentrated sulfuric acid
3: iron; aqueous acetic acid
4: H3aso4; aqueous H2SO4
View Scheme
参考文献
Case
Journal of Organic Chemistry, 1951 , vol. 16, p. 941,945
反应条件
1: iron; aqueous acetic acid
2: H3aso4; aqueous H2SO4
View Scheme
参考文献
Case
Journal of Organic Chemistry, 1951 , vol. 16, p. 941,945
反应条件
1: arsenic acid; concentrated sulfuric acid
2: iron; aqueous acetic acid
3: H3aso4; aqueous H2SO4
View Scheme
参考文献
Case
Journal of Organic Chemistry, 1951 , vol. 16, p. 941,945
反应条件
sulfuric acid; orthoarsenic acid
参考文献
Case
Journal of Organic Chemistry, 1951 , vol. 16, p. 941,945
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in tetrahydrofuran
Suzuki cross-coupling reaction; Heating;
参考文献
Ko, Chi-Chiu; Kwok, Wai-Ming; Yam, Vivian Wing-Wan; Phillips, David Lee
Chemistry - A European Journal, 2006 , vol. 12, # 22 p. 5840 - 5848
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane
T=70°C; Suzuki coupling;
参考文献
Kuehni, Joel; Adamo, Vincent; Belser, Peter
Synthesis, 2006 , # 12 p. 1946 - 1948
