N3-甲基吡啶-2,3-二胺合成路线 （共 16 条）
反应条件
1: tetrahydrofuran / 20 °C / |Inert atmosphere
2: acetic acid; iron / 3 h / 90 °C / |Inert atmosphere
View Scheme
参考文献
Sajith, Ayyiliath M.; Muralidharan, Arayambath; Karuvalam, Ranjith P.; Haridas, Karickal R.
Journal of the Korean Chemical Society, 2013 , vol. 57, # 3 p. 361 - 364
反应条件
1: tetrafluoroboric acid / toluene / 120 °C / |Inert atmosphere
2: tetrahydrofuran / 20 °C / |Inert atmosphere
3: acetic acid; iron / 3 h / 90 °C / |Inert atmosphere
View Scheme
参考文献
Sajith, Ayyiliath M.; Muralidharan, Arayambath; Karuvalam, Ranjith P.; Haridas, Karickal R.
Journal of the Korean Chemical Society, 2013 , vol. 57, # 3 p. 361 - 364
参考文献
Clark-Lewis; Thompson
Journal of the Chemical Society, <1957> 442, 446
参考文献
Plazek et al.
Roczniki Chemii, 1935 , vol. 15, p. 365,370
Chem. Zentralbl., 1936 , vol. 107, # I p. 1219
反应条件
in 1,2-dichloro-benzene
参考文献
USV Pharmaceutical Corporation
Patent: US4400382 A1, 1983 ;
反应条件
T=120°C; 24 h; Inert atmosphere;
参考文献
Sajith, Ayyiliath M.; Muralidharan, Arayambath; Karuvalam, Ranjith P.; Haridas, Karickal R.
Journal of the Korean Chemical Society, 2013 , vol. 57, # 3 p. 361 - 364
