反应条件
1.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere 2.1: triethylamine / dichloromethane / 8 h / 25 °C / Inert atmosphere 3.1: triphenylphosphine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere 3.2: 0 - 25 °C / Inert atmosphere 4.1: silver nitrate / acetonitrile / 6 h / Reflux; Inert atmosphere; Darkness 5.1: water / pH 7 - 8 / aq. phosphate buffer View Scheme
参考文献
Abdul-Hay, Samer; Schiefer, Isaac T.; Chandrasena, R. Esala P.; Li, Min; Abdelhamid, Ramy; Wang, Yue-Ting; Tavassoli, Ehsan; Michalsen, Bradley; Asghodom, Rezene T.; Luo, Jia; Thatcher, Gregory R. J.
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 9 p. 656 - 661
