反应条件
in toluene; Petroleum ether
Kinetics; byproducts: HCl, C2H6; (Ar); using Schlenk techniques; addn. of soln. of (C2H5)AlCl2 (12 equiv.) in petroleum ether to stirred suspn. of NdCl3*6H2O (1 equiv.) in toluene for 20 min at 40, 50, 70 and 90°C; stirring for 10 min; pptn., filtration, washing of solid twice with toluene and drying under vac., removal of solvent from filtrate in vac., elem. anal.;
参考文献
Bulgakov, Ramil G.; Kuleshov, Sergei P.; Zuzlov, Aleksei N.; Mullagaleev, Ildar R.; Khalilov, Leonard M.; Dzhemilev, Usein M.
Journal of Organometallic Chemistry, 2001 , vol. 636, # 1-2 p. 56 - 62
