2,3-二甲基-2-丁烯合成路线 (共 833 条)
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride T=20 - 35°C; 3 h; ultrasonic irradiation;
参考文献
Safiev, O. G.; Nazarov, D. V.; Zorin, V. V.; Rakhmankulov, D. L.; Paushkin, Ya. M.
Doklady Chemistry, 1988 , vol. 302, p. 280 - 282
Dokl. Akad. Nauk SSSR Ser. Khim., 1988 , vol. 302, # 3 p. 619 - 622
反应条件
1: t-BuOK / pentane / Ambient temperature 2: 96 percent / t-BuOK, DMSO / 4 h / Ambient temperature View Scheme
参考文献
Wijsman, G. W.; Wolf, W. H. de; Bickelhaupt, F.
Recueil des Travaux Chimiques des Pays-Bas, 1994 , vol. 113, # 1 p. 53 - 60
反应条件
N-bromosuccinmide; dihydrogen peroxide in diethyl ether Ambient temperature;
参考文献
Schulz, Manfred; Goermar, Gerhard; Lukac, Ivan
Journal fuer Praktische Chemie (Leipzig), 1990 , vol. 332, # 4 p. 491 - 495
反应条件
ozone in dichloromethane-d2 T=-85°C;
参考文献
McGarrity, John F.; Prodolliet, Jacques
Journal of Organic Chemistry, 1984 , vol. 49, # 23 p. 4465 - 4470
反应条件
ozone T=-254.16 - -238.16°C; 19 h; Inert atmosphere;
参考文献
Coleman, Bridgett E.; Ault, Bruce S.
Journal of Physical Chemistry A, 2010 , vol. 114, # 48 p. 12667 - 12674
反应条件
ozone in neat (no solvent) T=-247.2°C; activation energy, half life; Thermodynamic dataRate constant;
参考文献
Samuni; Haas; Fajgar; Pola
Journal of Molecular Structure, 1998 , vol. 449, # 2-3 p. 177 - 201
反应条件
in benzene-d6 72 h; Irradiation;
参考文献
Er, Erhan; Margaretha, Paul
Helvetica Chimica Acta, 1994 , vol. 77, p. 904 - 908
反应条件
1: HgCl2 / 45 - 50 °C 2: MgO; methanol / 200 °C 3: nickel Al2O3-kieselguhr; pentane / 160 °C / 73550.8 Torr / Hydrogenation View Scheme
参考文献
Universal Oil Prod.Co.
Patent: US2429373 , 1944 ;
反应条件
P=4.9 Torr; Irradiationdepends on present or absent and pressure of oxygene, NO and SF6; Product distributionQuantum yield;
参考文献
Collin, Guy J.; Deslauriers, Helene; Mare, George R. De
Canadian Journal of Chemistry, 1987 , vol. 65, p. 391 - 396
反应条件
hydrogenchloride; titanium(III) chloride; hydroxylamine hydrochloride; acetic acid
参考文献
Jung, Sang-Hun; Kohn, Harold
Tetrahedron Letters, 1984 , vol. 25, # 4 p. 399 - 402