2,3-二甲基-2-丁烯合成路线 (共 833 条)
反应条件
lithium aluminium tetrahydride; lt;CpCoNOgt;2; nitrogen(II) oxide 1) THF, 0 deg C, 85 min; 2) THF, -70 deg C, room temperature (overnight), reflux (1 h); Yield given. Multistep reaction;
参考文献
Michael; Carlson
Journal of Organic Chemistry, 1940 , vol. 5, p. 14,21
反应条件
in acetonitrile Irradiationreactions in var. solvents with several alkenes, with and without naphthalenes; intermediate of lifetime; MechanismQuantum yieldRate constant;
参考文献
Schuster, David I.; Brown, Pamela B.; Capponi, Louis J.; Rhodes, Christopher A.; Scaiano, J. C.; et al.
Journal of the American Chemical Society, 1987 , vol. 109, # 8 p. 2533 - 2534
反应条件
in acetonitrile 0.0833333 h; other olefines, N-oxides of amines, with water or with N,N-dimethylanline, var. temp., solv.; Product distributionMechanism;
参考文献
Zipplies, Matthias F.; Vos, Marie-Joelle De; Bruice, Thomas C.
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3228 - 3230
反应条件
Ru(CO)4I2 T=160°C; 3 h; Sealed tube;
参考文献
BP OIL INTERNATIONAL LIMITED
Patent: EP1900714 A1, 2008 ;
Location in patent: Page/Page column 4-6 ;
反应条件
T=520°C; KineticsProduct distribution;
参考文献
Koertvelyesi, Tamas; Seres, Laszlo
Journal of the Chemical Society, Faraday Transactions, 1992 , vol. 88, # 17 p. 2445 - 2450
反应条件
in benzene 5 h; Ambient temperatureIrradiation;
参考文献
Heterocycles, , vol. 27, # 10 p. 2417 - 2422
反应条件
4-methylbenzenesulfenyl chloride; lithium perchlorate in nitromethane T=20°C; 10 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 28, # 10 p. 1644 - 1650
Zhurnal Organicheskoi Khimii, , vol. 28, # 10 p. 2054 - 2062
反应条件
4-methylbenzenesulfenyl chloride; lithium perchlorate in nitromethane T=20°C; 10 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 28, # 10 p. 1644 - 1650
Zhurnal Organicheskoi Khimii, , vol. 28, # 10 p. 2054 - 2062
反应条件
4-methylbenzenesulfenyl chloride; lithium perchlorate in nitromethane T=20°C; 10 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 28, # 10 p. 1644 - 1650
Zhurnal Organicheskoi Khimii, , vol. 28, # 10 p. 2054 - 2062
反应条件
pyridine; dimethylsulfide in nitromethane
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 28, # 10 p. 1644 - 1650
Zhurnal Organicheskoi Khimii, , vol. 28, # 10 p. 2054 - 2062