2,3-二甲基-2-丁烯合成路线 (共 833 条)
反应条件
ozone P=4.1 Torr; 0.000777778 h; reaction in gas phase; mass spectrum of ozone and title compound; Product distributionMechanism;
参考文献
Martinez, Richard I.; Herron, John T.; Huie, Robert E.
Journal of the American Chemical Society, 1981 , vol. 103, # 13 p. 3807 - 3820
反应条件
ozone T=-254.16 - -238.16°C; 19 h; IrradiationInert atmosphere;
参考文献
Coleman, Bridgett E.; Ault, Bruce S.
Journal of Physical Chemistry A, 2010 , vol. 114, # 48 p. 12667 - 12674
反应条件
ozone in gaseous matrix T=24.9°C; P=700 Torr; examination of the formation of the secondary ozonides; variation of aldehyde partial pressure; study of addition of further aldehyde; Product distributionMechanism;
参考文献
Niki, H.; Maker, P. D.; Savge, C. M.; Breitenbach, L. P.; Hurley, M. D.
Journal of Physical Chemistry, 1987 , vol. 91, # 4 p. 941 - 946
反应条件
in trichloroethane, 1,1,1- T=-20°C; 15 h;
参考文献
Journal of the American Chemical Society, , vol. 118, # 20 p. 4778 - 4787
反应条件
1: concentrated aqueous H2SO4; acetic acid 2: AlCl3 View Scheme
参考文献
Wood,T.F. et al.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2248 - 2255
反应条件
DME*5HF T=20°C; 1 h;
参考文献
Bucsi, Imre; Toeroek, Bela; Marco, Alfonso Iza; Rasul, Golam; Prakash, G. K. Surya; Olah, George A.
Journal of the American Chemical Society, 2002 , vol. 124, # 26 p. 7728 - 7736
反应条件
in acetonitrile 1 h; Ambient temperatureIrradiation;
参考文献
Takechi, Haruko; Machida, Minoru; Kanaoka, Yuichi
Chemical & Pharmaceutical Bulletin, 1989 , vol. 37, # 5 p. 1431 - 1433
反应条件
T=-3.1 - 146.9°C; competitive edukt: 2-methyl-prop-1-en, various temp., influence of variation of reactants (further subst. ethenes) to isoselective temp.; Product distribution;
参考文献
Giese, Bernd; Lee, Woo-Bung
Angewandte Chemie, 1980 , vol. 92, # 10 p. 864 - 865
参考文献
Oda, Kazuaki; Machida, Minoru; Kanaoka, Yuichi
Heterocycles, 1984 , vol. 21, # 2 p. 622
反应条件
sodium hydroxide 0.7 h; Irradiationultrasound;
参考文献
Regen, Steven L.; Singh, Alok
Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1587 - 1588