2,3-二甲基-2-丁烯合成路线 (共 833 条)
反应条件
1: With tert.-butylhydroperoxide; Al tri-t-BuO- in benzene
T=20°C; 24 h;
2: With sulfuric acid in diethyl ether
Title compound not separated from byproducts;
参考文献
Martynova; Stepovik; Dodonov
Russian Journal of General Chemistry, 2001 , vol. 71, # 5 p. 736 - 741
反应条件
oxygen; silica gel; triphenylphosphine
T=30°C; 70 h; Irradiationchange the metal oxide, atmosphere, irradiation time; Product distribution;
参考文献
Gohre, Kirk; Miller, Glenn C.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1985 , vol. 81, p. 793 - 800
反应条件
trans,cis-Pt(PEt3)2Cl2(OH)(9-phenanthryl); oxygen in benzene-d6
Photolysis;
参考文献
Wickramasinghe, Lasantha A.; Sharp, Paul R.
Inorganic Chemistry, 2014 , vol. 53, # 3 p. 1430 - 1442
反应条件
trans,cis-Pt(PEt3)2(Cl)2(OH)(4-trifluoromethylphenyl) in dichloromethane-d2
0.0833333 h; PhotolysisInert atmosphere; Reagent/catalyst;
参考文献
Wickramasinghe, Lasantha A.; Sharp, Paul R.
Inorganic Chemistry, 2014 , vol. 53, # 3 p. 1430 - 1442
反应条件
trans,cis-Pt(PEt3)2(Cl)2(OH)(4-trifluoromethylphenyl) in chloroform-d1
0.0833333 h; PhotolysisInert atmosphere; Reagent/catalystSolvent;
参考文献
Wickramasinghe, Lasantha A.; Sharp, Paul R.
Inorganic Chemistry, 2014 , vol. 53, # 3 p. 1430 - 1442
反应条件
ozone in hexane
T=0°C; variation of concentration and temperature, other solvents or without solvent, addition of CH3CHO and phenanthrene; Product distributionMechanism;
参考文献
Murray, Robert W.; Kong, Wei; Rajadhyaksha, Shirish N.
Journal of Organic Chemistry, 1993 , vol. 58, # 2 p. 315 - 321
反应条件
trans,cis-Pt(PEt3)2Cl2(OH)(9-phenanthryl) in dichloromethane-d2
PhotolysisInert atmosphere;
参考文献
Wickramasinghe, Lasantha A.; Sharp, Paul R.
Inorganic Chemistry, 2014 , vol. 53, # 3 p. 1430 - 1442
反应条件
oxygen
T=60°C; P=759.8 Torr; 9 h;
参考文献
Bilas, W.; Hoebold, W.; Pritzkow, W.; Willecke, B.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 4 p. 682 - 686
反应条件
O(3P)
T=-42°C; Product distributionMechanism;
参考文献
Tanner; Kandanarachchi; Das; Brausen; Vo; Camaioni; Franz
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4587 - 4593
反应条件
lithium aluminium tetrahydride; oxygen
1.) 60 deg C, 9 h, 101.3 kPa;
参考文献
Bilas, W.; Hoebold, W.; Pritzkow, W.; Willecke, B.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 4 p. 682 - 686