2,3-二甲基-2-丁烯合成路线 (共 833 条)
反应条件
α-t-butyldimethylsilyloxyalkyl peroxybenzoate; palladium diacetate in dichloromethane
3 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Nagata, Ryu; Matsuura, Teruo; Saito, Isao
Tetrahedron Letters, 1984 , vol. 25, # 25 p. 2691 - 2694
反应条件
(2,3,7,8,12,13,17,18-octamethyl-5,10,15,20-tetraphenylporphinato)iron(III) chloride in dichloromethane
T=25°C; Product distribution;
参考文献
Woon, T. C.; Dicken, C. Michael; Bruice, Thomas C.
Journal of the American Chemical Society, 1986 , vol. 108, # 25 p. 7990 - 7995
反应条件
oxygen; silica gel; triphenylphosphine
T=30°C; 70 h; Irradiationchange the metal oxide, atmosphere, irradiation time; Product distribution;
参考文献
Gohre, Kirk; Miller, Glenn C.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1985 , vol. 81, p. 793 - 800
参考文献
O'Brien, Brian A.; Lam, William Y.; DesMarteau, Darryl D.
Journal of Organic Chemistry, 1986 , vol. 51, # 23 p. 4466 - 4470
反应条件
(TPPC2cap)FeIIISbF6 in dichloromethane
12 h; Ambient temperature; Mechanism;
参考文献
Dicken, C. Michael; Lu, Fu-Lung; Bruice, Thomas C.
Tetrahedron Letters, 1986 , vol. 27, # 49 p. 5967 - 5970
反应条件
phenyl(phenylazo)methyl hydroperoxide in benzene-d6
T=34°C; further hydroperoxides;
参考文献
Baumstark, A. L.; Vasquez, P. C.
Tetrahedron Letters, 1983 , vol. 24, # 2 p. 123 - 126
反应条件
in hexane
0.0522222 h;
参考文献
Murray, Robert W.; Kong, Wei; Rajadhyaksha, Shirish N.
Journal of Organic Chemistry, 1993 , vol. 58, # 2 p. 315 - 321
反应条件
oxygen in gas
T=69.9°C; P=200 Torr; 1.33333 h; Irradiationdifferent time, temperature and oxygen pressure; Product distribution;
参考文献
Morgan, Morag E.; Osborne, David A.; Waddington, David J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , p. 1869 - 1873
反应条件
ozone in hexane
T=0°C; variation of concentration and temperature, other solvents or without solvent, addition of CH3CHO and phenanthrene; Product distributionMechanism;
参考文献
Murray, Robert W.; Kong, Wei; Rajadhyaksha, Shirish N.
Journal of Organic Chemistry, 1993 , vol. 58, # 2 p. 315 - 321
反应条件
ozone
P=4.1 Torr; 0.000777778 h; reaction in gas phase; mass spectrum of ozone and title compound; Product distributionMechanism;
参考文献
Martinez, Richard I.; Herron, John T.; Huie, Robert E.
Journal of the American Chemical Society, 1981 , vol. 103, # 13 p. 3807 - 3820