2,3-二甲基-2-丁烯合成路线 (共 833 条)
反应条件
2,4,6-trimethylphenyl-dimethylamine; tin tetrabromide in 1,2-dichloro-ethane
T=60°C; 4 h;
参考文献
Nakyama; Nagase
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1878 - 1879
参考文献
Sumitomo Chemical Company, Limited
Patent: US5420356 A1, 1995 ;
反应条件
1: 7.7 g / Rh(OAc)4 / 12 h / 20 °C
2: KOH / methanol / 3 h / Heating
3: 0.702 g / tetrahydrofuran; diethyl ether / 2 h / -5 °C
View Scheme
参考文献
Thamattoor, Dasan M.; Snoonian, John R.; Sulzbach, Horst M.; Hadad, Christopher M.
Journal of Organic Chemistry, 1999 , vol. 64, # 16 p. 5886 - 5895
反应条件
potassium tert-butylate in pentane
参考文献
Doutheau,A.; Gore,J.
Bulletin de la Societe Chimique de France, 1976 , p. 1189 - 1194
反应条件
V-70L in chloroform-d1
T=25°C; 1 h; Darkness; Reagent/catalyst;
参考文献
Kita, Yasuyuki; Gotanda, Kentoku; Murata, Kenji; Suemura, Miki; Sano, Atsunori; Yamaguchi, Takahiro; Oka, Masahisa; Matsugi, Masato
Organic Process Research and Development, 1998 , vol. 2, # 4 p. 250 - 254
反应条件
(i) BH3, THF, (ii) hex-1-ene, (iii) /BRN= 3687486/; Multistep reaction;
参考文献
Arase,A.; Masuda,Y.
Chemistry Letters, 1976 , p. 1115 - 1118
反应条件
(i) BH3, THF, (ii) hex-1-ene, (iii) /BRN= 3912121/, aq. NH4<Fe(SO4)2>; Multistep reaction;
参考文献
Arase,A.; Masuda,Y.
Chemistry Letters, 1976 , p. 1115 - 1118
反应条件
in perdeuterocyclohexane
T=25°C; Irradiationother reactants: 3,4-diaza-2-methoxy-2-methyl-1-oxa<4.5>spirooct-3-ene, 2-methoxy-2,5,5-trimethyl-Δ3-1,3,4-oxadiazoline, various reactant ratios, other solvent: acetonitrile-d3; Product distributionMechanismRate constant;
参考文献
Pezacki; Pole; Warkentin; Chen; Ford; Toscano; Fell; Platz
Journal of the American Chemical Society, 1997 , vol. 119, # 13 p. 3191 - 3192
反应条件
[Ru2(CO)4(μ-OOC3H7)2]n in dichloromethane
T=20°C;
参考文献
Werle, Thorsten; Schaeffler, Lutz; Maas, Gerhard
Journal of Organometallic Chemistry, 2005 , vol. 690, # 24-25 p. 5562 - 5569
反应条件
aluminium trichloride
参考文献
Greuter,H.; Bellus,D.
Synthetic Communications, 1976 , vol. 6, p. 409 - 415